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Crystal data for 1a: C21H30N 1O4V1, Mr, 411.41, triclinic, space group P1̄ (No. 2, a, 9.1115(7, b, 9.7377(6, c, 14.1306(9)Å, a, 95.699(2)°, β= 91.858(3)°, γ, 113.789(5)°, V, 1137.9(1) Å3, Z, 2, T, 2.0 °C, Dcalcd, 1.201 g cm-3, μ(Mo Kα, 4.59 cm-1, MoKα radiation λ, 0.71069 Å, R1, 0.052, wR2, 0.150. CCDC-656969 for la. Crystal data for 1b: C18H21N 2O4V1, Mr, 380.32, monoclinic, space group P21 (No. 14, a= 10.9590(9, b, 10.8442(9, c, 15.2471(9)Å, β= 100.609(2)°, V, 1781.0(2)Aring;3, Z, 4, r, 4.0°C, Dcalcd, 1.418 gcm-3, μ(MoKα, 5.81 cm -1, MoKa radiation λ, 0.71069 Å, R1, 0.062, wR2, 0.172. CCDC-656970 for
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-1, MoKa radiation (λ = 0.71069 Å), R1 = 0.062, wR2 = 0.172. CCDC-656970 for lb.
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32
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0000310564
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is available electronically on the CSJJournal Web site
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Supporting Information is available electronically on the CSJJournal Web site, http://www.csj.jp/journals/chem-lett/.
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Supporting Information
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