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2 using the Siemens SHELXTL V 5.03 program package (PC version) (SHELXTL V5.03 program set; Siemens Analytical X-ray Instruments, Inc., Madison, WI, 1995).
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3, Z = 2, R1 = 0.043 (I > 2.0σ(I)), wR2 = 0.106, data-to-parameter ratio 6.7.
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85085782892
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3, Z = 4, R1 = 0.049 (I > 2.0σ(I)). wR2 = 0.126, data-to-parameter ratio 12.1.
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2NdSi: Nd, 26.04. Found: Nd, 26.66.
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