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37349060556
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4), filtered and evaporated yielding a crude product that was purified by flash chromatography (cyclohexane-EtOAc as eluent), giving the pure compound 6 or 7.
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4), filtered and evaporated yielding a crude product that was purified by flash chromatography (cyclohexane-EtOAc as eluent), giving the pure compound 6 or 7.
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23
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37349119929
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Selected Analytical Data for Compounds 6b,c and 7a,b: Compound 6b: yellow oil. IR (neat, 1456, 1916, 3354 cm-1. 1H NMR (400 MHz, CDCl3, δ, 0.86-0.92 (m, 3 H, 1.21-1.40 (m, 4 H, 1.60-1.93 (m, 3 H, 1.96-2.17 (m, 1 H, 2.32 (d, J, 8.1 Hz, 0.6 H, 2.45 (d, J, 4.3 Hz, 0.4 H, 2.65-2.80 (m, 1 H, 2.82-2.96 (m, 1 H, 3.82-3.94 (m, 0.6 H, 3.97-4.06 (m, 0.4 H, 4.40-4.49 (m, 1 H, 7.16-7.34 (m, 5 H, 13C NMR (100 MHz, δ, 13.9, 14.0, 22.3, 22.4, 27.9, 28.0, 28.3, 30.4, 31.8, 32.1, 35.0, 35.5, 71.4, 71.7, 92.5, 93.1, 126.5, 128.7, 128.8, 141.0. Anal. Calcd for C14H 21NO3: C, 66.91; H, 8.42; N, 5.57. Found: C, 67.24; H, 8.66; N, 5.38. Compound 6c: yellow oil. IR (neat, 1730, 3404 cm-1. 1H NMR (400 MHz, CDCl3, δ, 0.96-1.04 (m, 3 H, 1.37-1.94 (m, 5 H, 2.03-2.21 (m, 1 H, 2.43 (d, J, 7.7 Hz, 0.5 H, 2.54 d, J, 5.1
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5: C, 51.94; H, 7.41; N, 6.06. Found: C, 52.23; H, 7.61; N, 5.88.
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24
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0000283867
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