Determining Ten Synthetic Pyrethroids in Lettuce and Ground Meat by Using Ion-Trap Mass Spectrometry and Electron-Capture Gas Chromatography

Journal of Agricultural and Food Chemistry

Volumn 45, Issue 1, 1997, Pages 180-184

  Argauer, Robert J ^a   Eller, Konstantin I ^a   Pfeil, Richard M ^a   Brown, Richard T ^a  

^a AGRICULTURAL RESEARCH SERVICE   (United States)

Author keywords

Fat; Insecticides; Ion trap; Meat; SFE

Indexed keywords

LACTUCA;

EID: 0000471121     PISSN: 00218561     EISSN: None     Source Type: Journal    
DOI: 10.1021/jf960121b     Document Type: Article

References (19)

1. Argauer, R. J.; Eller, K. I.; Ibrahim, M. A.; and Brown, R. T. Determining propoxur and other carbamates in meat using HPLC-fluorescence and gas chromatography/ion trap mass spectrometry after supercritical fluid extraction. J. Agric. Food Chem. 1995, 43, 2774-2778.
2. Braun, H. E.; Stanek, J. Application of the AOAC multi-residue method of determination of synthetic pyrethroid residues in celery and animal products. J. Assoc. Off. Anal. Chem. 1982, 65, 685-689.
3. Chapman, R. A.; Harris, C. R. Extraction and liquid-solid chromatography cleanup procedures for the direct analysis of four pyrethroid insecticides in crops by gas-liquid chromatography. J. Chromatogr. 1978, 166, 513-518.
4. Code of Federal Regulations, Protection of Environment, 40, parts 150-189, revised July 1, 1992; Specific Tolerances 180.101-186.630.
5. Gere, D. R.; Derrico, E. M. SFE theory to practice-first principles and method development, Part 1, LC-GC 1994, 12, 352-366.
6. 2-A mini review. Food Chem. 1992, 45, 189-192.
7. Joia, B. S.; Webster, G. R. B.; Loschiavo, S. R. Cypermethrin and fenvalerate residues in stored wheat and milled fractions J. Agric. Food Chem. 1985, 33, 618-622.
8. Lee, D. W.; Westcott, N. D.; and Reichle, R. A. Gas-liquid chromatographic determination of pydrin, a synthetic pyrethroid, in cabbage and lettuce. J. Assoc. Off. Anal. Chem. 1978 61, 869-871.
9. Lehotay, S. J.; Eller, K. I. Development of a supercritical fluid extraction and gas chromatography/ion trap mass spectrometry method of analysis for 46 pesticides in fruits and vgetables. J. AOAC Int. 1995, 78, 821.
10. Murugaverl, B.; Gharaibeh, A.; Voorhees, K. J. Mixed adsorbent for cleanup during supercritical fluid extraction of three carbamate pesticides in tissues. J. Chromatogr. A 1993 657, 223-226.
11. Oehler, T. D. Gas liquid chromatographic determination of permethrin in bovine tissues. J. Assoc. Off. Anal. Chem. 1979, 62, 1309-1311.
12. Reichel, W. L.; Kolbe, E.; Stafford, C. J. Gas-liquid chromatographic and gas-liquid chromatographic-mass spectrometric determination of fenvalerate and permethrin residues in grasshoppers and duck tissue samples. J. Assoc. Off. Anal. Chem. 1981 64, 1196-1200.
13. Spittler, T. D.; Argauer, R. J.; Lisk, D. J.; Mumma, R. O.; and Winnett, G. Gas-liquid chromatographic determination of fenvalerate insecticide residues in processed apple products and by-products. J. Assoc. Off. Anal. Chem 1982, 65, 1106-1111.
14. Spittler, T. D.; Argauer, R. J.; Lisk, D. J; Mumma, R. O.; Winnett, G.; Ferro, D. N. Gas Chromatographic determination of fenvalerate insecticide residues in processed tomato products and by-products. J. Assoc. Off. Anal. Chem. 1984, 67, 824-826.
15. Synthetic Pyrethroids; ACS Symposium Series 42; Elliot, M., Ed.; American Chemical Society: Washington, DC, 1977.
16. Valverde-Garcia, A.; Fernandez-Alba, A. R.; Contreras, M.; Aguera, A. Supercritical fluid extraction of pesticides from vegetables using anhydrous magnesium sulfate for sample preparation. J. Agric. Food Chem. 1996, 44, 1780-1784.
17. Venant, A.; Van Neste, E.; Borrel, S.; Mallet, J. Determination of residues of deltamethrin in milk and butter. Food Addit. Contam. 1990, 7, 117-123.
18. Wei, L. Y. Determination of bifenthrin in pumpkins by gas chromatography and mass spectrometry Pestic. Sci. 1991, 32, 141-145.
19. Wszolek, P. C.; Lein, D. H.; Lisk, D. J. Excretion of fenvalerate insecticide in the milk of dairy cows. Bull. Environ. Contam. Toxicol. 1980, 24, 296-298.