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Volumn 72, Issue 24, 2007, Pages 9046-9052

An efficient preparation of new sulfonyl fluorides and lithium sulfonates

Author keywords

[No Author keywords available]

Indexed keywords

FLUORINATION; LITHIUM BATTERIES; LITHIUM COMPOUNDS; PHASE TRANSITIONS; SYNTHESIS (CHEMICAL);

EID: 36649006621     PISSN: 00223263     EISSN: None     Source Type: Journal    
DOI: 10.1021/jo701318n     Document Type: Article
Times cited : (73)

References (67)
  • 1
    • 7644227934 scopus 로고    scopus 로고
    • Xu, K. Chem. Rev. 2004, 104, 4303-4417.
    • (2004) Chem. Rev , vol.104 , pp. 4303-4417
    • Xu, K.1
  • 2
    • 0004145285 scopus 로고    scopus 로고
    • Wasserscheid, P, Welton, T, Eds, Wiley-VCH: Weinheim, Germany
    • Ionic Liquids in Synthesis; Wasserscheid, P., Welton, T., Eds.; Wiley-VCH: Weinheim, Germany, 2003.
    • (2003) Ionic Liquids in Synthesis
  • 5
    • 36648999297 scopus 로고    scopus 로고
    • Superacids; Olah, G. A., Prakash, G. K. S., Sommer J., Eds.; Wiley-Interscience: New York, 1984.
    • Superacids; Olah, G. A., Prakash, G. K. S., Sommer J., Eds.; Wiley-Interscience: New York, 1984.
  • 24
    • 36649037745 scopus 로고    scopus 로고
    • U.S. Patent 3420877 3M, 1969; Chem. Abstr. 1969, 70, 67609
    • (a) Pavlik, F. J. U.S. Patent 3420877 (3M), 1969; Chem. Abstr. 1969, 70, 67609.
    • Pavlik, F.J.1
  • 37
    • 36649009264 scopus 로고    scopus 로고
    • Takahashi, T.; Ichikawa, T.; Kanemaru, M.; Ishii, N. Mitsui Toatsu Chemicals Co. DE 2,241,807, 1973; Chem. Abstr. 1973, 78, 147341.
    • (a) Takahashi, T.; Ichikawa, T.; Kanemaru, M.; Ishii, N. Mitsui Toatsu Chemicals Co. DE 2,241,807, 1973; Chem. Abstr. 1973, 78, 147341.
  • 38
    • 36649034410 scopus 로고    scopus 로고
    • Tanaka, H.; Sako, N.; Oomura, T. Mitsubishi Chemical Industries Co. JP 6,199,504, 1994.
    • (b) Tanaka, H.; Sako, N.; Oomura, T. Mitsubishi Chemical Industries Co. JP 6,199,504, 1994.
  • 39
    • 36649013796 scopus 로고    scopus 로고
    • Holmes, C.; Pan, Y. Affimax, Inc. WO, 055026, 2002; Chem. Abstr. 2002, 137, 108891.
    • Holmes, C.; Pan, Y. Affimax, Inc. WO, 055026, 2002; Chem. Abstr. 2002, 137, 108891.
  • 40
    • 36649021044 scopus 로고    scopus 로고
    • U.S. Patent 013817, 107174
    • Lu, K. U.S. Patent 013817, 2003; Chem. Abstr. 2003, 138, 107174.
    • (2003) Chem. Abstr , vol.138
    • Lu, K.1
  • 42
    • 36649003225 scopus 로고    scopus 로고
    • Ballad-Longeau, A.; Pereira, F.; Capron, P.; Mercier, R. C.E.A. FR 2843399, 2004; Chem. Abstr. 2004, 140, 166774.
    • Ballad-Longeau, A.; Pereira, F.; Capron, P.; Mercier, R. C.E.A. FR 2843399, 2004; Chem. Abstr. 2004, 140, 166774.
  • 43
    • 36649036073 scopus 로고    scopus 로고
    • Ferreira, L.; Blakeney, J. A.; Spaziano, G. D.; Dimov, O.; Kocab, T. J.; Hatfield, J. P. Arch. Spec. Chem., Inc. WO, 02,082,185, 2002; Chem. Abstr. 2002, 137, 317924.
    • Ferreira, L.; Blakeney, J. A.; Spaziano, G. D.; Dimov, O.; Kocab, T. J.; Hatfield, J. P. Arch. Spec. Chem., Inc. WO, 02,082,185, 2002; Chem. Abstr. 2002, 137, 317924.
  • 44
    • 36649020596 scopus 로고    scopus 로고
    • Doyle, M. C.; Feiring, A. E.; Choi, S. K. DuPont WO, 9,967,-304, 1999; Chem. Abstr. 1999, 132, 50411.
    • (a) Doyle, M. C.; Feiring, A. E.; Choi, S. K. DuPont WO, 9,967,-304, 1999; Chem. Abstr. 1999, 132, 50411.
  • 47
    • 36649005095 scopus 로고    scopus 로고
    • Adachi, K.; Ishihara, S.; Kuroki, Y.; Itagaki, T. Daikin Industries, Ltd. WO, 072,021, 2004; Chem. Abstr. 2004, 141, 206920.
    • Adachi, K.; Ishihara, S.; Kuroki, Y.; Itagaki, T. Daikin Industries, Ltd. WO, 072,021, 2004; Chem. Abstr. 2004, 141, 206920.
  • 56
    • 36649023231 scopus 로고    scopus 로고
    • As our work was under completion, a patent from DuPont (WO, 113491, 2005) appeared in the literature that presented the synthesis of compound 2c; however, the reported synthesis is less efficient than ours because the potassium salt of the thiolate was isolated and needed to be carefully dried, and because 2c was apparently obtained in a crude 88.5% yield. Our approach does not need to isolate the thiolate, and our isolated yield is higher.
    • As our work was under completion, a patent from DuPont (WO, 113491, 2005) appeared in the literature that presented the synthesis of compound 2c; however, the reported synthesis is less efficient than ours because the potassium salt of the thiolate was isolated and needed to be carefully dried, and because 2c was apparently obtained in a crude 88.5% yield. Our approach does not need to isolate the thiolate, and our isolated yield is higher.
  • 57
    • 36648999296 scopus 로고    scopus 로고
    • University of Southern California WO, 03048033, 2003
    • (a) Prakash, G. K. S.; Hu, J.; Olah, G. A. University of Southern California WO, 03048033, 2003; Chem. Abstr. 2003, 139, 23755.
    • (2003) Chem. Abstr , vol.139 , pp. 23755
    • Prakash, G.K.S.1    Hu, J.2    Olah, G.A.3
  • 62
    • 36649004010 scopus 로고    scopus 로고
    • Similar sulfonyl chlorides are claimed in a patent from Daikin Industries, Ltd, see ref 23, However, no ArSCF2SO2Cl was exemplified
    • 2Cl was exemplified.
  • 63
    • 36649015733 scopus 로고    scopus 로고
    • 2Br) as precursor which has to be isolated, transformed into the sulfonyl chloride, and then transformed into the corresponding sulfonyl fluoride through an halogene exchange reaction. Our approach is more general, much simpler and is carried out in the same pot.
    • 2Br) as precursor which has to be isolated, transformed into the sulfonyl chloride, and then transformed into the corresponding sulfonyl fluoride through an halogene exchange reaction. Our approach is more general, much simpler and is carried out in the same pot.
  • 64
    • 36649016157 scopus 로고    scopus 로고
    • Sanchez, J.-Y.; Langlois, B.; Médebielle, M.; Toulgoat, F. FR 0606466, 2006.
    • Sanchez, J.-Y.; Langlois, B.; Médebielle, M.; Toulgoat, F. FR 0606466, 2006.
  • 66
    • 36649031149 scopus 로고    scopus 로고
    • Sanchez, J.-Y.; Paillard, E.; Iojoiu, C.; Alloin, F.; Toulgoat, F.; Médebielle, M.; Langlois, B. FR 0606471, 2006.
    • (a) Sanchez, J.-Y.; Paillard, E.; Iojoiu, C.; Alloin, F.; Toulgoat, F.; Médebielle, M.; Langlois, B. FR 0606471, 2006.
  • 67
    • 36649003796 scopus 로고    scopus 로고
    • Sanchez, J.-Y.; Paillard, E.; Iojoiu, C.; Alloin, F.; Toulgoat, F.; Médebielle, M.; Langlois, B. FR 0606469, 2006.
    • (b) Sanchez, J.-Y.; Paillard, E.; Iojoiu, C.; Alloin, F.; Toulgoat, F.; Médebielle, M.; Langlois, B. FR 0606469, 2006.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.