4-Amino- and 4-nitrodipicolinatovanadium(V) complexes and their hydroxylamido derivatives: Synthesis, aqueous, and solid-state properties

Inorganic Chemistry

Volumn 46, Issue 23, 2007, Pages 9827-9840

  Smee, Jason J ^a,b   Epps, Jason A ^a   Teissedre, Guillaume ^a   Maes, Mandy ^a   Harding, Nichola ^a   Yang, Luqin ^a   Baruah, Bharat ^a   Miller, Susie M ^a   Anderson, Oren P ^a   Willsky, Gail R ^c   Crans, Debbie C ^a  

^a Department of Environmental and Radiological Health Sciences   (United States)

^b UNIVERSITY OF TEXAS AT TYLER   (United States)

^c UNIVERSITY AT BUFFALO   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

AMIDE; DIPICOLINIC ACID; PICOLINIC ACID DERIVATIVE; VANADIUM DERIVATIVE; WATER;

ARTICLE; CHEMICAL STRUCTURE; CHEMISTRY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SOLUBILITY; SYNTHESIS;

AMIDES; MAGNETIC RESONANCE SPECTROSCOPY; MODELS, MOLECULAR; PICOLINIC ACIDS; SOLUBILITY; VANADIUM COMPOUNDS; WATER;

EID: 36348996465     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic701233y     Document Type: Article

References (64)

1. Crans, D. C.; Smee, J. J. In Comprehensive Coordination Chemistry, 2nd ed.; McCleverty, J., Meyer, T. J., Eds.; Elsevier: Oxford, 2003; Vol. 4, 175-239.
2. Vilas Boas, L. V.; Costa Pessoa, J. In Comprehensive Coordination Chemistry. The Synthesis, Reactions, Properties & Applications of Coordination Compounds; Wilkinson, G., Sir, Gillard, R. D., McCleverty, J. A., Eds.; Pergamon Press: New York, 1987; Vol. 3, pp 453-583.
3. Rehder, D. Inorg. Chem. Commun. 2003, 6, 604-617.
4. Tracey, A. S.; Willsky, G. R.; Takeuchi, E. S. Vanadium: Chemistry, Biochemistry, Pharmacology and Practical Applications; CRC Press: Boca Raton, FL, U.S.A., 2007.
5. Gaetjens, J.; Meier, B.; Kiss, T.; Nagy, E. M.; Buglyo, P.; Sakurai, H.; Kawabe, K.; Rehder, D. Chem.-Eur. J. 2003, 9, 4924-4935.
6. Davies, D. R.; Ho, W. G. J. FEBS Lett. 2004, 577, 315-321.
7. Borden, J.; Crans, D., C.; Florian, J. J. Phys. Chem. B 2006, 110, 14988-14999.
8. Crans, D. C.; Keramidas, A. D.; Drouza, C. Phosphorus, Sulfur Silicon Relat. Elem. 1996, 109-110, 245-248.
9. Crans, D. C.; Smee, J. J.; Gaidamauskas, E.; Yang, L. Chem. Rev. 2004, 104, 849-902.
10. Hakansson, K.; Lindahl, M.; Svensson, G.; Albertsson, J. Acta Chem. Scand. 1993, 47, 449-455.
11. Okabe, N.; Oya, N. Acta Crystallogr., Sect. C: Cryst. Struct. Commun. 2000, C56, 305-307.
12. Laine, P.; Gourdon, A.; Launay, J.-P. Inorg. Chem. 1995, 34, 5138-5149.
13. Crans, D. C.; Smee, J. J.; Gaidamauskiene, E. G.; Anderson, O. P.; Miller, S. M.; Jin, W.-Z.; Gaidamauskas, E.; Crubellier, E.; Grainda, R.; Chi, L. H.; Willsky, G. R. J. Inorg. Biochem. 2004, 98, 1837-1850.
14. MacDonald, J. C.; Luo, T.-J. M.; Palmore, G. T. R. Cryst. Growth Des. 2004, 4, 1203-1209.
15. Mukherjee, P. S.; Das, N.; Kryschenko, Y. K.; Arif, A. M.; Stang, P. J. J. Am. Chem. Soc. 2004, 126, 2464-2473.
16. Brayshaw, P. A.; Hall, A. K.; Harrison, W. T. A.; Harrowfield, J. M.; Pearce, D.; Shand, T. M.; Skelton, B. W.; Whitaker, C. R.; White, A. H. Eur. J. Inorg. Chem. 2005, 1127-1141.
17. Sukanya, D.; Prabhakaran, R.; Natarajan, K. Polyhedron 2006, 25, 2223-2228.
18. Manohar, T. C.; Rajkumar, M.; Rajagopal, S. Transition Met. Chem. (Dordrecht, Neth.) 2006, 31, 549-555.
19. Mauk, A. G.; Bordignon, E.; Gray, H. B. J. Am. Chem. Soc. 1982, 104, 7654-7657.
20. Holder, A. A.; Brown, R. F. G.; Marshall, S. C.; Payne, V. C. R.; Cozier, M. D.; Alleyne, W. A.; Bovell, C. O. Transition Met. Chem. (Dordrecht, Neth.) 2000, 25, 605-611.
21. Crans, D. C.; Yang, L.; Jakusch, T.; Kiss, T. Inorg. Chem. 2000, 39, 4409-4416.
22. Buglyo, P.; Crans, D. C.; Nagy, E. M.; Lindo, R. L.; Yang, L.; Smee, J. J.; Jin, W.; Chi, L.-H.; Godzala, M. E., III; Willsky, G. R. Inorg. Chem. 2005, 44, 5416-5427.
23. Nuber, B.; Weiss, J.; Wieghardt, K. Z. Naturforsch., B: Chem. Sci. 1978, 33B, 265-267.
24. Yang, L.; La Cour, A.; Anderson, O. P.; Crans, D. C. Inorg. Chem. 2002, 41, 6322-6331.
25. Crans, D.; Mahroof-Tahir, M.; Johnson, M.; Wilkins, P.; Yang, L.; Robbins, K.; Johnson, A.; Alfano, J.; Godzala, M.; Austin, L.; Willsky, G. Inorg. Chim. Acta 2003, 356, 365-378.
26. Gonzalez-Baro, A. C.; Castellano, E. E.; Piro, O. E.; Parajon-Costa, B. S. Polyhedron 2005, 24, 49-55.
27. Bersted, B. H.; Belford, R. L.; Paul, I. C. Inorg. Chem. 1968, 7, 1557-1562.
28. Sundheim, A.; Mattes, R. Z. Naturforsch., B: Chem. Sci. 1993, 48B, 125-132.
29. Chatterjee, M.; Ghosh, S.; Nandi, A. Transition Met. Chem. (Dordrecht, Neth.) 1999, 24, 183-185.
30. Chatterjee, M.; Maji, M.; Ghosh, S.; Mak, T. C. W. J. Chem. Soc., Dalton Trans. 1998, 3641-3645.
31. Drew, R. E.; Einstein, F. W. B. Inorg. Chem. 1973, 12, 829-835.
32. Mimoun, H.; Chaumette, P.; Mignard, M.; Saussine, L. Nouv. J. Chim. 1983, 7, 467-475.
33. Nuber, B.; Weiss, J. Acta Crystallogr., Sect. B: Struct. Sci. 1981, B37, 947-948.
34. Slebodnick, C.; Hamstra, B. J.; Pecoraro, V. L. Struct. Bonding 1997, 89, 51-108.
35. Rehder, D.; Casny, M.; Grosse, R. Magn. Reson. Chem. 2004, 42, 745-749.
36. Butler, A.; Clague, M. J.; Meister, G. Chem. Rev. 1994, 94, 625-638.
37. Schwendt, P.; Sivak, M. In Vanadium Compounds: Biochemistry, Chemistry, and Therapeutic Applications; Tracey, A. S., Crans, D. C., Eds.; Oxford University Press: 1998; pp 117-125.
38. Wieghardt, K. Adv. Inorg. Org. Bioinorg. Mech. 1984, 3, 213-274.
39. Paul, P. C.; Angus-Dunne, S. J.; Batchelor, R. J.; Einstein, F. W. B.; Tracey, A. S. Can. J. Chem. 1997, 75, 429-440.
40. Angus-Dunne, S. J.; Paul, P. C.; Tracey, A. S. Can. J. Chem. 1997, 75, 1002-1010.
41. Nxumalo, F.; Tracey, A. S. J. Biol. Inorg. Chem. 1998, 3, 527-533.
42. Bhattacharyya, S.; Martinsson, A.; Batchelor, R. J.; Einstein, F. W. B.; Tracey, A. S. Can. J. Chem. 2001, 79, 938-948.
43. Paul, P. C.; Angus-Dunne, S. J.; Batchelor, R. J.; Einstein, F. W. B.; Tracey, A. S. Can. J. Chem. 1997, 75, 183-191.
44. Keramidas, A. D.; Miller, S. M.; Anderson, O. P.; Crans, D. C. J. Am. Chem. Soc. 1997, 119, 8901-8915.
45. Wieghardt, K. Inorg. Chem. 1978, 17, 57-64.
46. Bradshaw, J. S.; Maas, G. E.; Lamb, J. D.; Izatt, R. M.; Christensen, J. J. J. Am. Chem. Soc. 1980, 102, 467-74.
47. Lewis, J. C. J. Biol. Chem. 1972, 247, 1861-1868.
48. Robison, M. M. J. Am. Chem. Soc. 1958, 80, 5481-5483.
49. Sheldrick, G. M. SADABS (a Program for Siemens Area Detection Absorption Correction); 2000.
50. Sheldrick, G. M. SHELXTL Siemens Analytical X-ray Diffraction; Siemens: Madison, WI, 1996.
51. 2) at acidic pH (1-2) at 80°C as depicted in Scheme 1 to form complexes 1-3. Thus, the increased temperature is necessary to assure that all the dipicolinic acid (or its derivatives) dissolves. Because of the tendency to form decavanadate under the intermittent reaction conditions the preparation of the hydroxylamido complexes is most reliably obtained beginning from the dipicolinate complexes 1-3.
52. Addison, A. W.; Rao, T. N. J. Chem. Soc., Dalton Trans. 1984, 1349-1356.
53. Tinant, B.; Bayot, D.; Devillers, M. Z. Kristallogr. - New Cryst. Struct. 2003, 218, 477-478.
54. Tracey, A. S.; Gresser, M. J.; Galeffi, B. Inorg. Chem. 1988, 27, 157-161.
55. Funahashi, S.; Haraguchi, K.; Tanaka, M. Inorg. Chem. 1977, 16, 1349-1353.
56. 10 is a major problem in preparation of these complexes, the concentrations are low, and the binary complexes are sufficiently stable that this species does not significantly impact these studies.
57. Rehder, D.; Wieghardt, K. Z. Naturforsch., B: Chem. Sci. 1981, 36b, 1251-1254.
58. Bissot, T. C.; Parry, R. W.; Campbell, D. H. J. Am. Chem. Soc. 1957, 79, 796-800.
59. Cornman, C. R.; Colpas, G. J.; Hoeschele, J. D.; Kampf, J.; Pecoraro, V. L. J. Am. Chem. Soc. 1992, 114, 9925-9933.
60. 3 stock solution should not be adjusted below ∼7 prior to mixing, or else the reaction will be seriously compromised.
61. Nxumalo, F.; Tracey, A. S. J. Biol. Inorg. Chem. 1998, 3, 527-533.
62. Wavefunction, Inc.: Irvine, CA, 2006.
63. Ooms, K. J.; Boite, S. E.; Smee, J. J.; Baruah, B.; Crans, D. C.; Polenova, T. Inorg. Chem. 2007, 46, in press.
64. Hartkamp, H. Angew. Chem. 1959, 71, 553.