Cu[(PPh3)2O](acac): Cu+ charge-compensated by a coordinating acac- anion

Inorganic Chemistry Communications

Volumn 10, Issue 12, 2007, Pages 1561-1564

  Xie, Yi Ming ^a   Wu, Ji Huai ^a  

^a HUAQIAO UNIVERSITY   (China)

Author keywords

Copper; Crystal structure; Diketone; Photoluminescence

Indexed keywords

EID: 36248999922     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2007.09.027     Document Type: Article

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15. Synthesis of the title complex: The acac (1 mmol, 0.100 g) was added to a mixture of metallic copper powder (1 mmol, 0.064 g) and bis(2-diphenyl-phosphinophenyl) ether (1 mmol, 0.538 g) in 20 mL acetone. The mixture was stirred at room temperature for 48 h giving a white precipitate. The product was collected by filtration and washed with acetone. Colorless crystals were obtained by recrystallization of the product from methanol and ether. The crystals are stable in air. Yield: 86% (based on copper powder).
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