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34
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85030944307
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note
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One of the acetone molecules was treated with disorder. Due to high thermal parameters, the acetones were restrained to be flat, with similar C-C and C=O distances.
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35
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85030938245
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note
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- anion was also located with high disorder of the F atoms and only four F atoms were located.
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36
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85030935328
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note
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- anions were restrained to be in octahedral geometry with F atoms around the P atom and similar P-F bond lengths and thermal parameters; (ii) phenyl rings were restrained to be normal hexagonal rings with bond lengths of 1.39 Å; (iii) some C atoms have unexpectedly high thermal parameters, atoms in the phenyl rings concerned were restrained to have the same thermal parameters; (iv) some extra individual restraints had to be applied to prevent unusual structure.
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