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Volumn 46, Issue 43, 2007, Pages 8246-8249

An alkylidyne analogue of Tebbe's reagent: Trapping reactions of a titanium neopentylidyne by incomplete and complete 1,2-additions

Author keywords

Alkylidenes; Alkylidynes; Aluminum; N,P ligands; Titanium

Indexed keywords

CHEMICAL BONDS; COMPLEXATION; LIGANDS; PYRIDINE; REACTION KINETICS;

ALKYLIDENES; TITANIUM NEOPENTYLIDYNE; TRAPPING REACTIONS;

TITANIUM COMPOUNDS;

EID: 36049009338 PISSN: 14337851 EISSN: None Source Type: Journal
DOI: 10.1002/anie.200703079 Document Type: Article

Times cited : (34)

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- See Supporting Information for complete experimental details.

20
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- Crystal data for 2: C34H58AlNP 2Ti, Mr, 617.63, triclinic, space group P1, a, 10.9247(8, b, 11.6164(8, c, 14.3622(10) Å, α, 93.013(2, β, 97.780(2, γ, 97.587(2)°, Z, 2, μ, 0.376 mm-1, MoKα, 0.71073 Å, V, 1785.4(2) Å3, T, 125(2)°C, ρcalcd, 1.149 mg mm-3, GoF on F2, 1.031, R 1, 3.39% and wR2, 8.25, F2, all data, Out of a total of 45767 reflections collected, 8215 were unique and 7094 were observed (Rint, 4.82, with I > 2σI red-pink prism, 0.30 x 0.30 x 0.20 mm3, 27.48° ≥ Θ ≥ 2.2°, A direct-methods solution was calculated which provided most non-hydrogen atoms from the E-map. Full-matrix least squares/differe
- [15]

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25
- 36048937680
- Crystal data for 5: C34H58BNO 3P2Ti·0.25C5H12, Mr, 686.73, monoclinic, space group P2 1/n, a, 11.5558(6, b, 21.5062(11, c, 16.1661(8) Å, β, 106.3710(10)°, Z, 4, μ, 0.339 mm-1, MoKα, 0.71073 Å, V, 3854.7(3) Å3, T, 125(2)°C, ρcalcd, 1.183 mg mm-3, GoF on F2, 1.103, R1, 6.39% and wR2, 12.20, F2, all data, Out of a total of 114062 reflections collected, 8834 were unique and 6839 were observed (Rint, 6.25, with I > 2σI red-brown block, 0.25 x 0.25 x 0.25 mm3, 24.80° ≥ Θ ≥ 2.23°, A direct-methods solution was calculated which provided most non-hydrogen atoms from the E-map. Fu
- [15]

26
- 36048983483
- CCDC-650732 (2) and CCDC-650733 (5) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.
- CCDC-650732 (2) and CCDC-650733 (5) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.

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