SCOPUS 정보 검색 플랫폼

Volumn 9, Issue 21, 2007, Pages 4203-4206

First desymmetrization of 1,3-propanediamine derivatives in organic solvent. Development of a new route for the preparation of optically active amines

(5) Bustos, Eduardo a Gotor Fernández, Vicente a Montejo Bernardo, Jose a García Granda, Santiago a Gotor, Vicente a

a UNIVERSITY OF OVIEDO (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

AMINE; DIAMINE; LIPASE B, CANDIDA ANTARCTICA; SOLVENT; TRIACYLGLYCEROL LIPASE; UNCLASSIFIED DRUG;

ARTICLE; CATALYSIS; CHEMICAL STRUCTURE; CHEMISTRY; CONFORMATION; METABOLISM; STEREOISOMERISM; SYNTHESIS; X RAY CRYSTALLOGRAPHY;

AMINES; CATALYSIS; CRYSTALLOGRAPHY, X-RAY; DIAMINES; LIPASE; MOLECULAR CONFORMATION; MOLECULAR STRUCTURE; SOLVENTS; STEREOISOMERISM;

EID: 35548970395 PISSN: 15237060 EISSN: None Source Type: Journal
DOI: 10.1021/ol701720m Document Type: Article

Times cited : (27)

References (19)

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19
- 35548989160
- Colorless crystal, crystal dimensions 0.22 × 0.06 × 0.02 mm3; C24H27F3N2O 4 (Mr, 464.48, monoclinic, space group P21, a, 13.1146, 15) Å, b, 9.4909(6) Å, c, 19.586(3) Å, β= 103.373(15)°, V, 2371.7(5) Å3, Z, 2, Dx= 1.301 Mg m-3, μ, 0.882 mm-1. λ, 1.54180 Å(Cu Kα, Data collection at 100(2) K, 2θmax, 104.62°, 7935 measured reflections and 4192 independent reflections (Rint 0.070, Final value of R1 (F2 > 2σ(F2, 0.0521, wR2 (F2 > 2σF2, 0.0877. Residual electron density 0.216/-0.220 e Å-3. Data collection was made using the program CrysAlis CCD. Crystal structure was solved by direct methods using the program Sir2004. Anisotropic least-squares refinement was carried out with SHELX
- -3. Data collection was made using the program CrysAlis CCD. Crystal structure was solved by direct methods using the program Sir2004. Anisotropic least-squares refinement was carried out with SHELXL-97. Absolute configuration was determined as R,R from the Friedel Pairs and the reference of one known center. Structure details were deposited at the CSD database (CCDC-651954 Cambridge).

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