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Crystallographic data of compound 1: C25H22N 2O6, M, 446.51, orthorhombic, space group P222, a, 9.8873 (16) Å, b, 11.8185 (19) Å, c, 20.1890 (3) Å, a, 90.000, β, 90.000, γ, 90.000, V, 2359.2 (7) Å3, Z, 4. Crystal dimensions 0.09 × 0.21 × 0.38 mm3 were used for measurements on a MAC DIP-2030K diffractometer with a graphite monochromator (ω scan, 2θ max, 56.74, Mo Kα radiation. The total number of independent reflections measured was 15 384, of which 5539 were observed, F|2 ≥ 2σ|F|2, Final indices: Rf= 0.0579, wR2, 0.1220 (w, 1/σ|F|2, S, 1.004. The crystal structure (1) was solved by the direct method SHELXS-97, expanded using geometrical calculations and difference Fourier techniques, and refined by l
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2), S = 1.004. The crystal structure (1) was solved by the direct method SHELXS-97, expanded using geometrical calculations and difference Fourier techniques, and refined by least-squares calculations. Crystallographic data for the structure of compound 1 have been deposited in the Cambridge Crystallographic Date Centre (deposition number: CCDC 652447). Copies of these data can be obtained free of charge via http:/www.ccdc.cam.ac.uk/deposit (or from Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge CB2 1EZ, U.K., Facsimile: (44) 01223 336033, e-mail: deposit@ccdc.cam.ac.uk).
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