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Volumn 46, Issue 20, 2007, Pages 8108-8110

A "cation-less" oxalate-based ferromagnet formed by neutral bimetallic layers: {[Co(H2O)2]3[Cr(ox) 3]2(18-crown-6)2}∞ (ox = Oxalate dianion; 18-crown-6 = C12H24O6)

(3) Coronado, Eugenio a Galán Mascarós, José R a Martí Gastaldo, Carlos a

a UNIVERSITY OF VALENCIA (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 35348851383 PISSN: 00201669 EISSN: None Source Type: Journal
DOI: 10.1021/ic700808h Document Type: Article

Times cited : (28)

References (31)

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- 2O (2 mmol; 0.48 g) were suspended in 5 mL of methanol. The solution was stirred for 15 min, and the AgCl precipitate was removed from the dark violet solution. This mixture was carefully poured into one H-tube leg, while 18-crown-6 (1 mmol; 0.264 g) was added in the other. The diffusion tube was filled with MeOH and left to stand. After 10 days, the dark blue prismatic crystals that grew in one of the tube legs were filtered, washed with MeOH, and dried in air. Anal. Calcd (Found) for (1): C, 29.91 (29.63); H, 4.18.
- 2O (2 mmol; 0.48 g) were suspended in 5 mL of methanol. The solution was stirred for 15 min, and the AgCl precipitate was removed from the dark violet solution. This mixture was carefully poured into one H-tube leg, while 18-crown-6 (1 mmol; 0.264 g) was added in the other. The diffusion tube was filled with MeOH and left to stand. After 10 days, the dark blue prismatic crystals that grew in one of the tube legs were filtered, washed with MeOH, and dried in air. Anal. Calcd (Found) for (1): C, 29.91 (29.63); H, 4.18.

29
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- Data were collected with a Nonius Kappa CCD diffractometer using graphite-monochromated Mo Kα radiation (λ, 0.71073) at 293 K. The structure was solved by direct methods (SIR97, followed by Fourier synthesis, and refined on F2 (SHELXL-97, The non-hydrogen atoms were refined anisotropically. C36H60Co 3Cr2O42, Mw, 1445.63, orthorhombic, Pc21n a, 14.3950(4) Å, b, 15.6500(5) Å, c, 26.6700(10) Å, V, 6008.3(3) Å3, T, 293(2) K, Z, 4, ρcalcd, 1.598 g/cm3, F(000, 2964, μ= 1.265 mm-1, 27596 reflections, 7937 unique (Rint, 0.1070, 2θ max, 22.74°, R(F, 0.0615, and R w(F2, 0.1497 for 5581 reflections [I>2σI, CCDC 635244 contains suppl
- 2) - 0.1497 for 5581 reflections [I>2σ(I)]. CCDC 635244 contains supplementary crystallographic data for this paper. It can be obtained free of charge via www.ccdc.cam.ac.uk/retrieving.html.

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