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Volumn 46, Issue 19, 2007, Pages 7692-7694

Spin transition at the mesophase transition temperature in a cobalt(II) compound with branched alkyl chains

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EID: 34948822273 PISSN: 00201669 EISSN: None Source Type: Journal
DOI: 10.1021/ic700754s Document Type: Article

Times cited : (69)

References (21)

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- The ligand C5C12C10-terpy was synthesized by mixing 5-decyl-1- bromoheptadecane (1.57 g, 3.43 mmol, 2,6-bis(2-pyridyl)-4(1H)-pyridone (0.57 g, 2.29 mmol, and K2CO3 (0.63 g, 4.58 mmol) in N,N-dimethylformamide (70 mL) at 80°C for 12 h. 1H NMR (CDCl3, 0.88 (t, J, 7.0 Hz, 3H, 1.25-1.55 (m, 47H, 1.85 (q, J, 7.3 Hz, 2H, 4.23 (t, J, 6.3 Hz, 2H, 7.32 (td, J, 6.8 Hz, 2H, 7.86 (td, J, 8.5 Hz, 2H, 8.01 (s, 2H, 8.61 (d, J, 8.0 Hz, 2H, 8.68 (d, J, 6.0 Hz, 2H, The cobalt(II) compound 1 was synthesized by mixing C5C12C10-terpy (0.44 mmol, 0.28 g) and Co(BF4)2·6H2O (0.23 mmol, 0.078 g) in CHCl3/MeOH (30 mL, The obtained brown powder was collected by filtration and recrystallized from acetone/EtOH yield: 188 mg, 55, Anal. Calcd for C84H130N6O2B 2F8
- 1: C, 67.78; H, 8.80; N, 5.65. Found: C, 67.83; H, 8.82; N, 5.72.

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- A geometry optimization for the compounds was performed in the gas phase by using Chem3D Ultra 10.0.

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