Characterization of (13C24) T-2 toxin and its use as an internal standard for the quantification of T-2 toxin in cereals with HPLC-MS/MS

Analytical and Bioanalytical Chemistry

Volumn 389, Issue 3, 2007, Pages 931-940

  Haubl G ^a   Berthiller, F ^a   Hametner, C ^b   Rechthaler, J ^c   Jaunecker, G ^d   Freudenschuss, M ^d   Krska, R ^a   Schuhmacher, R ^a  

^a UNIVERSITY OF NATURAL RESOURCES AND LIFE SCIENCES   (Austria)

^b VIENNA UNIVERSITY OF TECHNOLOGY   (Austria)

^c UNIVERSITY OF APPLIED SCIENCES WIENER NEUSTADT   (Austria)

^d Biopure Referenzsubstanzen GmbH   (Austria)

Author keywords

Internal standard; Isotope dilution; Maize; Mass spectrometry; Oat; T 2 toxin

Indexed keywords

CROPS; DILUTION; GRAIN (AGRICULTURAL PRODUCT); ISOTOPES; MASS SPECTROMETRY; SUBSTITUTION REACTIONS;

INTERNAL STANDARDS; ISOTOPE DILUTION; MAIZE; OAT;

TOXIC MATERIALS;

AVENA; ZEA MAYS;

CARBON; T 2 TOXIN;

ARTICLE; CEREAL; CHEMISTRY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ISOTOPE DILUTION ASSAY; MAIZE; MASS SPECTROMETRY; METHODOLOGY; OAT; REPRODUCIBILITY; SENSITIVITY AND SPECIFICITY; STANDARD;

AVENA SATIVA; CARBON ISOTOPES; CEREALS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; MASS SPECTROMETRY; RADIOISOTOPE DILUTION TECHNIQUE; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; T-2 TOXIN; ZEA MAYS;

EID: 34648814362     PISSN: 16182642     EISSN: 16182650     Source Type: Journal    
DOI: 10.1007/s00216-007-1493-7     Document Type: Article

References (28)

1. Bamburg JR, Riggs NV, Strong FM (1968) Tetrahedron 24:3329-3336
2. Bennet JW, Klich M (2003) Clin Microbiol Rev 16:497-516
3. Joint FAO/WHO Expert Committee on Food Additives (JECFA) (2001) FAO Food and Nutrition Paper 74. FAO/WHO, Geneva (see http://www.inchem.org/documents/ jecfa/jecmono/v47je01.htm, cited 18 July 2007)
4. Moss MO, Thrane U (2004) Toxicol Lett 153:23-28
5. EC (2006) Regulation 1881/2006. Off J Eur Union L364:5
6. EC (2006) Recommendation 576/2006. Off J Eur Union L229:7
7. Krska R, Baumgartner S, Josephs R (2001) Fresenius J Anal Chem 371:285-299
8. Koch P (2004) Toxicol Lett 153:109-112
9. Ler SG, Lee FK, Gopalakrishnakone P (2006) J Chromatogr A 1133:1-12
10. Visconti A, Lattanzio VMT, Pascale M, Haidukowski M (2005) J Chromatogr A 175:151-158
11. Tanaka H, Takino M, Sugita-Konishi Y, Tanaka T (2006) Rapid Commun Mass Spectrom 20:1422-1428
12. Biancardi A, Gasparini M, Dall'Asta C, Marchelli R (2005) Food Addit Contam 22:251-258
13. Berthiller F, Schuhmacher R, Buttinger G, Krska R (2005) J Chromatogr A 1062:209-216
14. Biselli S, Hummert C (2005) Food Addit Contam 22:752-760
15. Cavaliere C, Foglia P, Pastorini E, Samperi R, Lagana A (2005) Rapid Commun Mass Spectrom 19:2085-2093
16. Sulyok M, Berthiller F, Krska R, Schuhmacher R (2006) Rapid Commun Mass Spectrom 20:2649-2659
17. Wallace EM, Pathre SV, Mirocha CJ, Robison TS, Fenton SW (1977) J Agric Food Chem 25:836-838
18. Hagler WM, Mirocha CJ, Pathre SV (1981) Appl Environ Microbiol 41:1049-1051
19. Michaud DP, Karger BL, Vouros P (1988) J Label Comp Radiopharm 25:345-348
20. Pawlosky RJ, Mirocha CJ, Wen Y, Abbas HK (1989) J Assoc Off Anal Chem 72:807-812
21. Asam S, Rychlik M (2006) J Agric Food Chem 54(18):6535-6546
22. Wegscheider W, Rohrer C, Neuböck R (1999) Validata: MS Excel macro for method validation, Ver. 3.02.48. Wegscheider-Rohrer-Neuböck, Leoben, Austria
23. Blackwell BA, Greenhalgh R, Bain AD (1984) J Agric Food Chem 32:1078-1083
24. Mesilaakso M, Moilanen M, Rahkamaa E (1989) Arch Environ Contam Toxicol 18:365-373
25. Savard ME, Blackwell BA (1994) In: Miller JD, Trenholm HL (eds) Mycotoxins in grain. Eagan, St. Paul, MN, USA
26. Häubl G, Berthiller F, Rechthaler J, Jaunecker G, Binder EM, Krska R, Schuhmacher R (2006) Food Addit Contam 23:1187-1193
27. EURACHEM/CITAC Guide (2000) Quantifying uncertainty in analytical measurement, 2nd edn. EURACHEM, Teddington, UK (see http://www.eurachem.org/ guides/QUAM2000-1.pdf, cited 18 July 2007)
28. Swanson SP, Ramaswamy V, Beasley VR, Buck, WB, Burmeister HH (1983) J AOAC Int 66 (4):909-912