Self-assembly of a Co4III face-shared partial double cubane supported by alkoxo terminal and bridging ligands

Inorganic Chemistry Communications

Volumn 10, Issue 10, 2007, Pages 1202-1205

  Mandal, Debashree ^a   Ray, Debashis ^a  

^a INDIAN INSTITUTE OF TECHNOLOGY   (India)

Author keywords

Bis tridentate; Di cubane; Di Schiff base; Methoxo bridge; Tetranuclear; X ray structure

Indexed keywords

EID: 34548632935     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2007.07.006     Document Type: Article

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35. -3. Precise unit cell dimensions were determined from the least squares refinement of 25 well-centered reflections having 2θ values in 1.78-24.97° range. The systematic absences are 0 ⇐ h ⇐ 9, -14 ⇐ k ⇐ 14, -14 ⇐ l ⇐ 15. The intensities of three reference reflections of each complex was monitored every one-hour though out the data collection shows no sign of crystal deterioration. The structure was solved by direct method SHELXS-97 [31], followed by successive Fourier synthesis and least-square refinement using SHELXS-97 program [32]. Direct phase determination yielded Co, and most of the C, N, O atoms. Anisotropic thermal parameters are used for the nonhydrogen atoms and isotropic parameters for the hydrogen atoms.
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