Influence of hydrothermal synthesis temperature on the structures of two 3D coordination polymers

Inorganic Chemistry Communications

Volumn 10, Issue 10, 2007, Pages 1198-1201

  Wang, Fang Kuo ^a   Song, Xiu Xian ^a   Yang, Shi Yao ^a   Huang, Rong Bing ^a   Zheng, Lan Sun ^a  

^a XIAMEN UNIVERSITY   (China)

Author keywords

Coordination polymer; Crystal structure; Hydrothermal synthesis; Temperature

Indexed keywords

EID: 34548616883     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2007.07.008     Document Type: Article

References (22)

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20. 5, found (calcd) C 36.93 (37.09), H 2.95 (2.91)%.
21. 2 = 0.0625. The detail crystallographic data for 1 and 2 have been deposited at the Cambridge Crystallographic Data Center as supplementary publication CCDC No. 650134 & 650135.
22. Selected bond lengths (Å) and angles (°) for 1: Zn-O 1.927(3), 1.942(3), O-Zn-O: 99.33(17), 109.71(13), 117.73(11), 103.37(18). 2: Zn1-O1 2.124(1), Zn1-O6 2.055(2), Zn1-O7 2.058(1), Zn1-O8 2.036(1), Zn1-O1b 2.170(1), Zn1-O3a 2.056(1), Zn2-O7 2.073(1), Zn2-O2b 2.140(1), Zn2-O8b 2.130(1), Zn3-O5 1.922(2), Zn3-O7 1.967(1), Zn3-O4e 1.925(2), Zn3-O8d 1.974(1) Å; O1-Zn1-O7 86.54(5), O1-Zn1-O8 91.05(5), O1-Zn1-O1b 80.17(5), O1-Zn1-O3a 94.10(6), O6-Zn1-O7 92.58(6), O6-Zn1-O8 89.42(6), O6-Zn1-O1b 88.55(6), O6-Zn1-O3a 97.13(7), O7-Zn1-O3a 86.63(6), O7-Zn1-O1b 91.02(5), O8-Zn1-O1b 86.73(5), O8-Zn1-O3a 95.41(6), O7-Zn2-O2b 95.66(5), O7-Zn2-O2d 84.34(5), O7-Zn2-O8b 98.18(5), O7-Zn2-O8d 81.82(5), O7c-Zn2-O2b 84.34(5), O7c-Zn2-O2d 95.66(5), O7c-Zn2-O8b 81.82(5), O7c-Zn2-O8d 98.18(5), O8b-Zn2-O2b 96.84(5), O8b-Zn2-O2d 83.16(5), O8d-Zn2-O2b 83.16(5), O8d-Zn2-O2d 96.84(5), O5-Zn3-O7 111.71(6), O5-Zn3-O4e 103.41(7), O5-Zn3-O8d 121.37(7), O7-Zn3-O8d 88.63(5), O7-Zn3-O4e 123.29(7), O4e-Zn3-O8d 109.45(6), Zn1-O1-Zn1b 99.83(5), Zn1-O7-Zn2 118.05(6), Zn1-O7-Zn3 116.48(7), Zn2-O7-Zn3 95.82(6), Zn1-O8-Zn2f 117.96(6), Zn1-O8-Zn3f 118.36(7), Zn2f-O8-Zn3f 93.80(6). Symmetry codes: (a) -x + 1, y - 1/2, -z + 3/2; (b) -x + 1, -y + 1, -z + 1; (c) -x, -y + 1, -z + 1; (d) x - 1, y, z; (e) -x, y - 1/2, -z + 3/2; (f) x + 1, y, z.