Analysis of trace amounts of carbon dioxide, oxygen and carbon monoxide in nitrogen using dual capillary columns and a pulsed discharge helium ionisation detector

Journal of Chromatography A

Volumn 1167, Issue 1, 2007, Pages 102-108

  Janse van Rensburg, M ^a   Botha, A ^a   Rohwer, E ^b  

^a NATIONAL METROLOGY INSTITUTE OF SOUTH AFRICA   (South Africa)

^b UNIVERSITY OF PRETORIA   (South Africa)

Author keywords

Carbon dioxide; Carbon monoxide; Nitrogen; Oxygen; Uncertainty; Validation

Indexed keywords

CARBON DIOXIDE; CARBON MONOXIDE; GAS DETECTORS; OXYGEN; UNCERTAINTY ANALYSIS;

PARALLEL DUAL CAPILLARY COLUMNS; PULSED DISCHARGE HELIUM IONISATION DETECTION (PDHID);

GAS MIXTURES;

CARBON DIOXIDE; CARBON MONOXIDE; HELIUM; NITROGEN; OXYGEN;

ANALYTIC METHOD; ARTICLE; DEVICE; FLOW RATE; GAS ANALYSIS; GAS CHROMATOGRAPHY; INTERMETHOD COMPARISON; IONIZATION; MEASUREMENT; PRIORITY JOURNAL; TEMPERATURE;

CARBON DIOXIDE; CARBON MONOXIDE; CHROMATOGRAPHY, GAS; CHROMATOGRAPHY, GEL; ELECTROPHORESIS, CAPILLARY; HELIUM; NITROGEN; OXYGEN; OXYGEN INHALATION THERAPY; SENSITIVITY AND SPECIFICITY; TEMPERATURE;

EID: 34548485791     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2007.07.055     Document Type: Article

References (27)

1. International Standard ISO Guide 34, General requirements for the competence of reference material producers, International Organization for Standardization (ISO), Geneva, 2003.
2. Novelli P.C. Chemosphere: Global Change Sci. 1 (1999) 115
3. Kaminski M., Kartanowicz R., Jastrzebski D., and Kaminski M.M. J. Chromatogr. A 989 (2003) 277
4. Porter K., and Volman D.H. Anal. Chem. 34 (1962) 748
5. 2 in Ethylene and Propylene, Application Note 26, Varian, Palo Alto, CA, 2006; http://www.varianinc.com/media/sci/apps/gc26.pdf.
6. International Standard ISO 8186, Ambient Air - Determination of the Mass Concentration of Carbon Monoxide - Gas Chromatographic Method, International Organization for Standardization (ISO), Geneva, 1989.
7. 2 in Nitrogen NML-06-006, CSIR NML Technical Output Database, Pretoria, 2006.
8. M. Janse van Rensburg, Validation of GC-TCD/FID Method for Determination of CO in Nitrogen NML-06-010, CSIR NML Technical Output Database, Pretoria, 2006.
9. Andrawes F.F., and Gibson Jr. E.K. Anal. Chem. 51 (1979) 3
10. 2 by Using a Parallel Setup of Optimized PLOT Columns, Application Note, Varian, The Netherlands, 2007; http://www.varianinc.com/image/vimage/docs/products/consum/gccolumns/select/shared/P152_Select_Perm_Gas.pdf.
11. Restek, Chromatography Products Catalogue, Restek, Bellefonte, PA, 2004-2005, p. 649.
12. Wurm D.B., Sun K., and Winniford W.L. J. Chromatogr. Sci. 41 (2003) 545
13. Miller J.N., and Miller J.C. Statistics and Chemometrics for Analytical Chemistry. 4th ed. (2000), Prentice Hall, Harlow p. 124
14. Wentworth W.E., Cai H., and Stearns S. J. Chromatogr. A 688 (1994) 135
15. Forsyth D.S. J. Chromatogr. A 1050 (2004) 63
16. In: Hogan J.D. (Ed). Speciality Gas Analysis: A Practical Guidebook (1997), Wiley-VCH, New York 53
17. Thompson B. Fundamentals of Gas Analysis by Gas Chromatography (1977), Varian, Palo Alto, CA p. 10
18. International Standard ISO 6142, Gas Analysis - Preparation of Calibration Gas Mixtures - Gravimetric Method, International Organisation for Standardization (ISO), Geneva, 1998.
19. Sandra P. J. High Resolut. Chromatogr. 12 (1989) 273
20. Dyson N.A. Chromatographic Integration Methods (1990), Royal Society of Chemistry, Great Britain p. 98
21. Currie L.A. Anal. Chim. Acta 391 (1999) 105
22. Eurachem Guide, The Fitness for Purpose of Analytical Methods: A Laboratory Guide to Method Validation and Related Topics, Geneva, 1998; http://www.eurachem.ul.pt/guides/valid.pdf, viewed 2005.
23. Huber W. Accred. Qual. Assur. 8 (2003) 213
24. W. Bremser, B_LEAST, Bundesamsalt for Materialforschung Und Prüfung (BAM), Berlin, 1997.
25. International Standard ISO 6143, Gas Analysis - Determination of Composition and Checking of Calibration Gas Mixtures, International Organisation for Standardization (ISO), Geneva, 1997.
26. Guide to the Expression of Uncertainty in Measurement, International Standards Organization (ISO), Geneva, 1993.
27. Eurachem/CITAC Guide, Quantifying Uncertainty in Analytical Measurement, 2nd ed., Geneva, 1995; http://www.measurementuncertainty.org/mu/guide/, viewed 2005.