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Volumn 26, Issue 17, 2007, Pages 4115-4117

Peripheral functionalization of diruthenium compounds via heck reactions

Author keywords

[No Author keywords available]

Indexed keywords

COORDINATION REACTIONS; ELECTRONIC PROPERTIES; PERTURBATION TECHNIQUES; REACTION KINETICS; RUTHENIUM COMPOUNDS; VOLTAMMETRY;

COORDINATION COMPOUNDS; CROSS-COUPLING REACTIONS; DIRUTHENIUM COMPOUNDS; HECK REACTIONS;

ORGANOMETALLICS;

EID: 34548188268 PISSN: 02767333 EISSN: None Source Type: Journal
DOI: 10.1021/om7005408 Document Type: Article

Times cited : (13)

References (29)

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- Preparation of la. To a suspension of Pd(OAc)2 (ca. 0.1 equiv) in Et3N were added Ru2(D(3,5-Cl2Ph)F) 3(D(4-IPh)F)Cl (0.40 g) and styrene (5-10 equiv, The resultant mixture was refluxed under N2 overnight. The product purification was effected via extraction and flash chromatography to yield 0.20 g of la (52, ESI-MS (mle, based on 101Ru, 1600, corresponding to [M, Cl, Anal. Found (caled) for C68H48Cl 13N8Ru2: C, 48.91 (49.92, H, 2.73 (2.71, N, 6.63 6.85
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- 2-THF: C, 46.12 (46.25); H, 2.89 (2.98); N, 7.02 (7.19).

25
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- Preparation of 3a. A mixture of frani-(C 2Ph)2-Ru2(D(3,5-Cl2Ph)F) 3(DMBA-I, 0.080 g, styrene (10 equiv, KF (2 equiv, nBu 4NCl (3 equiv, Pd(dba)2 (0.1 equiv, and toluene (20 mL) was stirred under N2 overnight for 4 days. The product purification was effected by recrystallization to yield 0.050 g of 3a (60, ESI-MS (mle, based on 101Ru, 1652, M, 1H NMR: 8.16 (s, IH, NCHN, 8.00 (s, 2H, NCHN, 7.85-7.81 (d, 2H, aromatic, 7.61-7.57 (d, 2H, aromatic, 7.46-6.61 (m, 35H, aromatic and vinyl H, 3.67 s, 6H, NCH3
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