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1H NMR spectrum of the crude product, and the stereochemistry was assigned by nuclear Overhauser effect studies. It was further confirmed after deprotection to sMGPs; the glycosidic protons of β-linked anomers are known to give resonances shifted to upfields compared to those of the corresponding α-linked anomers.
-
1H NMR spectrum of the crude product, and the stereochemistry was assigned by nuclear Overhauser effect studies. It was further confirmed after deprotection to sMGPs; the glycosidic protons of β-linked anomers are known to give resonances shifted to upfields compared to those of the corresponding α-linked anomers.
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