메뉴 건너뛰기




Volumn 129, Issue 32, 2007, Pages 9862-9863

Total synthesis of methyl sarcophytoate

Author keywords

[No Author keywords available]

Indexed keywords

METHYL SARCOPHYTOATE; NATURAL PRODUCT; UNCLASSIFIED DRUG;

EID: 34547917936     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja073952e     Document Type: Article
Times cited : (30)

References (25)
  • 13
    • 33947274308 scopus 로고    scopus 로고
    • Synthetic studies by Xu's group:, and references therein
    • Synthetic studies by Xu's group: Yao, H.; Gao, Y.; Liu, P.; Sun, B.; Xu, X. Synlett 2007, 571 and references therein.
    • (2007) Synlett , pp. 571
    • Yao, H.1    Gao, Y.2    Liu, P.3    Sun, B.4    Xu, X.5
  • 15
    • 2142858450 scopus 로고    scopus 로고
    • Enantiomeric excess was determined by the modified Mosher ester analysis: Ohtani, I.; Kusumi, T.; Kashman, Y.; Kakisawa, H. J. Am. Chem. Soc. 1991, 113, 4092. For absolute configuration, see Supporting Information.
    • Enantiomeric excess was determined by the modified Mosher ester analysis: Ohtani, I.; Kusumi, T.; Kashman, Y.; Kakisawa, H. J. Am. Chem. Soc. 1991, 113, 4092. For absolute configuration, see Supporting Information.
  • 19
    • 34547914265 scopus 로고    scopus 로고
    • Structure determination of 11a and 11b is in Supporting Information.
    • Structure determination of 11a and 11b is in Supporting Information.
  • 23
    • 34547911175 scopus 로고    scopus 로고
    • The 4Z-isomer structure was determined by precise NMR analysis. See Supporting Information.
    • The 4Z-isomer structure was determined by precise NMR analysis. See Supporting Information.
  • 24
    • 34547888476 scopus 로고    scopus 로고
    • The starting materials were recovered (2: 39%, 15: 30%). The longer the reaction time, the lower the isolated yield due to partial decompositions. Other thermal conditions: in toluene, rt, 4 days, no reaction; in toluene, 60°C, 2.5 days, partial decomposition of 15; in 1,2-dichlorobenzene, 140°C, 1 day, decomposition of 2 and 15.
    • The starting materials were recovered (2: 39%, 15: 30%). The longer the reaction time, the lower the isolated yield due to partial decompositions. Other thermal conditions: in toluene, rt, 4 days, no reaction; in toluene, 60°C, 2.5 days, partial decomposition of 15; in 1,2-dichlorobenzene, 140°C, 1 day, decomposition of 2 and 15.
  • 25
    • 3042745794 scopus 로고    scopus 로고
    • Review for the enzymatic Diels-Alder reaction: Oikawa, H.; Tokiwano, T. Nat. Prod. Rep. 2004, 21, 321.
    • Review for the enzymatic Diels-Alder reaction: Oikawa, H.; Tokiwano, T. Nat. Prod. Rep. 2004, 21, 321.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.