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34547852934
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note
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C{double bond, long}C). Notes: Perchlorate salts of metal complexes are potentially explosive and should be handled with care.
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42
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note
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int = 0.0167). Structure solution and refinement based on 3101 observed reflections with I > 2σ(I) and 308 parameters gave final R = 0.0479, wR = 0.1212 and S = 1.002. All of the calculations were performed by the SHELXTL™TM 5 program. Crystallographic data in cif format have been deposited with the Cambridge Crystallographic Data Center, CCDC No. 609058 for 1 and 609285 for 2.
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