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34547845720
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note
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6): C, 60.40; H, 4.19; N, 14.57%. Found: C, 59.98; H, 4.18; N, 14.55%.
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18
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34547834563
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note
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2 = 0.1366, S = 1.047, completeness is 99.8%. The X-ray intensity data were measured at 213(2) K on a Bruker SMART 1000 CCD detector with a Mo-target X-ray tube (λ = 0.71073 Å). Data reduction and integration were performed using the software SAINTPLUS. Absorption corrections were applied using the program SADABS. The structures was solved by direct methods and refined using the SHELXL-97 program. Subsequent cycles of least-squares refinement followed by difference Fourier syntheses revealed the positions of the remaining non-hydrogen atoms. Hydrogen atoms were added at calculated positions based on a riding model.
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33751005225
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note
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It should be noted that to attach compounds of this type to microelectrodes, it would be necessary to have a linker with two sulfur atoms, e.g., benzene dithiolate.
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