Determination of glycerol in wines using 31P-NMR spectroscopy

JAOCS, Journal of the American Oil Chemists' Society

Volumn 84, Issue 7, 2007, Pages 615-619

  Hatzakis, Emanuel ^a   Archavlis, Eleftherios ^a   Dais, Photis ^a  

^a UNIVERSITY OF CRETE   (Greece)

Author keywords

31P NMR spectroscopy; Glycerol; Wine

Indexed keywords

DERIVATIVES; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; STATISTICAL METHODS; WINE;

BLAND AND ALTMAN STATISTICAL ANALYSIS; DERIVATIZATION; HYDROXYL GROUPS;

GLYCEROL;

EID: 34547480797     PISSN: 0003021X     EISSN: None     Source Type: Journal    
DOI: 10.1007/s11746-007-1099-4     Document Type: Article

References (16)

1. Nieuwoudt H, Prior B, Pretorius I, Bauer F (2002) Glycerol and wine quality: fact and fiction. Wynboer 9:96-101
2. Lubbers S, Verrer C, Voilley A (2001) The effect of glycerol on the perceived aroma of a model wine and a white wine. Lebensm Wiss U Tecnol 34:262-265
3. Fernandes EN, de Campos Moura MN, Costa Lima JLF, Reis BF (2004) Automatic flow procedure for the determination of glycerol in wine using enzymatic reaction and spectrophotometry. Microchem J 77:107-112
4. Cuadrado MU, Luque de Castro MD, Perez Juan PM, Gomez-Nieto MA (2005) Comparison and joint use of near infrared spectroscopy and Fourier transform mid infrared spectroscopy for the determination of wine parameters. Talanta 66:218-224
5. AOAC Official methods of analysis (1998) Glycerol in wine and grape juice mono and diglycerides in fats and oils. Gas chromatographic method, 16th ed. Official methods of analysis of AOAC international, Gaithersburg, Maryland, vol 2. Chapter 41, pp 46-49
6. Callul M, Marce RM, Borrull F (1992) Determination of carboxylic acids, sugars, glycerol and ethanol in wine and grape must by ion-exchange high performance liquid chromatography with refractive index detection. J Chromatogr 590:215-222
7. Kosir IJ, Kidric J (2002) Use of modern nuclear magnetic resonance spectroscopy in wine analysis: determination of minor compounds. An Chim Acta 458:77-84
8. Calderone G, Naulet N, Guillou C, Reniero F (2004) Characterization of European wine glycerol: stable carbon isotope approach. J Agric Food Chem 52:5902-5908
9. 31P-NMR spectroscopy in food analysis. Quantitative determination of the mono and diglyceride composition of olive oils. J Agric Food Chem 48:802-805
10. 31P-NMR spectroscopy. J Agric Food Chem 54:656-664
11. 31P-NMR spectroscopy. J Agric Food Chem 50:2207-2213
12. Zwierzak A (1967) Cyclic organophosphorus compounds. I. Synthesis and infrared spectral studies of cyclic hydrogen phosphites and thiophosphites. Can J Chem 45:2501-2512
13. Sanchez Munoz G, Garcia Romero E, Perez Coello MS, Martin Alvarez PJ (1992) Determination of glycerol in wines by high performance liquid chromatography: comparison with enzymatic method. J Chromatogr 623:43-47
14. Water quality-calibration and evaluation of analytical methods and estimation of performance characteristics (1990) Part 1:Statistical evaluation of the linear calibration function, ISO Norm 8466-1
15. Bland JM, Altman DG (1986) Statistical methods for assessing agreement between two methods of clinical measurements. Lancet 1:307-310
16. Pollock MA, Jefferson SG, Kane JW, Lomax K, MacKinnon G, Winnard CB (1992) Method comparison: a different approach. Ann Clin Biochem 29:556-560