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Volumn , Issue 20, 2007, Pages 3169-3172

Electron density and bonding in borates: An experimental study of tetrabutylammonium heptahydridohexaborate, [(C4H9) 4N][B6H7]

Author keywords

Borates; Charge density; Topological analysis

Indexed keywords

ATOMS; TOPOLOGY;

EID: 34547166426     PISSN: 14341948     EISSN: 10990682     Source Type: Journal    
DOI: 10.1002/ejic.200700444     Document Type: Article
Times cited : (19)

References (32)
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    • Crystals of [Bu4N][B6H7] were obtained by crystallization from methanol. Empirical formula:, C4H 94N][B6H7, formula mass [gmol -1, 314.37; crystal system: monoclinic; space group: P21/ n (no. 14, Z, 4; temperature: 98 K; cell parameters: a, 8.611(1) Å, b, 17.112(2) Å, c, 15.151(2) Å, β, 99.309(5)°, V, 2203.1(5) Å3; density: 0.9478(2) g cm-3; λ, 0.71073 Å; 2θmax, 102.85°; 162395 reflections, 23027 unique reflections; completeness: 92.0, redundancy: 7.0; R(F2)int, 0.039, R(F)mul, 0.026; residual density: -0.16/0.21 eÅ-3. CCDC-637977 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic
    • -3. CCDC-637977 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.
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