Characterization of components of nano-energetics by small-angle scattering techniques

Journal of Materials Research

Volumn 22, Issue 7, 2007, Pages 1907-1920

  Mang, Joseph T ^a   Hjelm, Rex P ^a   Son, Steven F ^a   Peterson, Paul D ^a   Jorgensen, Betty S ^a  

^a LOS ALAMOS NATIONAL LABORATORY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

AGGREGATE GEOMETRY; LOG-NORMAL DISTRIBUTION; MAXIMUM ENTROPY ALGORITHM; NANO-ENERGETIC MATERIALS; SURFACE LAYER THICKNESS;

AGGLOMERATION; DENSITY (SPECIFIC GRAVITY); FRACTAL DIMENSION; MORPHOLOGY; NANOPARTICLES; NEUTRON SCATTERING; PARTICLE SIZE ANALYSIS; X RAY SCATTERING;

POWDERS;

EID: 34547119949     PISSN: 08842914     EISSN: None     Source Type: Journal    
DOI: 10.1557/jmr.2007.0230     Document Type: Article

References (42)

1. R.P. Hjelm, W.A. Wampler, P.A. Seeger, and M. Gerspacher: The microstructure and morphology of carbon black: A study using small angle neutron scattering and contrast variation. J. Mater. Res. 9, 3210 (1994).
2. L.F. Shen, A. Stachowiak, S.E.K. Fateen, P.E. Laibinis, and T.A. Hatton: Structure of alkanoic acid stabilized magnetic fluids: A small angle neutron and light scattering analysis. Langmuir 17, 288 (2001).
3. x, removal catalysts. Physica B (Amsterdam) 241-243, 269 (1998).
4. T. Lowe: The revolution in nanometals. Adv. Mater. Proc. 160, 63 (2002).
5. S.F. Son, J.R. Busse, B.W. Asay, P.D. Peterson, J.T. Mang, B. Bockman, and M.L. Pantoya: Propagation studies of metastable intermolecular composites (MIC), in Proceedings of the 29th International Pyrotechnics Seminar, edited by F.J. Schelling (International Pyrotechnics Seminars, IPS USA, Inc., Marshall, TX, 2002), p. 203.
6. S.F. Son, M.A. Hiskey, D.L. Naud, J.R. Busse, and B.W. Asay: Lead-free electric matches, in Proceedings of the 29th International Pyrotechnics Seminar, edited by F.J. Schelling (International Pyrotechnics Seminars, IPS USA, Inc., Marshall, TX, 2002), p. 871.
7. S.M. Walley, J.E. Balzer, W.G. Proud, and J.E. Field: Response of thermites to dynamic high pressure and shear. Proc. R. Soc. London A 456, 1483 (2000).
8. B. Jorgensen (unpublished).
9. B.S. Bockmon. M.L. Pantoya, S.F. Son, B.W. Asay, and J.T. Mang: Combustion velocities and propagation mechanisms of metastable interstitial composites. J. Appl. Phys. 98, 064903 (2005).
10. L.I. Espada, J.T. Mang, E.B. Orler, D.A. Wrobleski, D.A. Langlois, and R.P. Hjelm: Structural characterization of segmented polyurethanes by small angle neutron scattering, in Polymer Interfaces and Thin Films, edited by A. Karim, T.P. Russell, C.W. Frank, and P.F. Nealey (Mater. Res. Soc. Symp. Proc. 710, Warrendale, PA, 2002), p. 193.
11. J.T. Koberstein, B. Morra, and R.S. Stein: Determination of diffuse-boundary thicknesses of polymers by small-angle x-ray scattering. J. Appl. Crystallogr. 13, 34 (1980).
12. G. Beaucage: Small-angle scattering from polymeric mass fractals of arbitrary mass-fractal dimension. J. Appl. Crystollogr. 29, 134 (1996).
13. G.S. Iannacchione, C.W. Garland, J.T. Mang, and T.P. Rieker: Calorimetric and small angle x-ray scattering study of phase transitions in octylcyanobiphenyl-aerosil dispersions. Phys. Rev. E 58, 5966 (1998).
14. J.T. Mang, S. Kumar, and B. Hammouda: Discotic micellar nematic and lamellar phases under shear flow. Europhys. Lett 28, 489 (1994).
15. R.P. Hjelm, C. Schteingart, A.F. Hofmann, and D.S. Sivia: Form and structure of self-assembling particles in monoolein-bile salt mixtures. J. Phys. Chem. 99, 16395 (1995).
16. P. Thiyagarajan: Characterization of materials of industrial importance using small-angle scattering techniques. J. Appl. Crystallogr. 36, 373 (2003).
17. K.C. Littrell, N.R. Khalili, M. Campbell, G. Sandi, and P. Thiyagarajan: Microstructural analysis of activated carbons prepared from paper mill sludge by SANS and BET. Chem. Mater, 14, 327 (2002).
18. J.T. Mang, C.B. Skidmore, R.P. Hjelm, and P,M. Howe: Application of small-angle neutron scattering to the study of porosity in energetic materials. J. Mater. Res. 15, 1199 (2000).
19. G. Fagherazzi and S. Polizzi: Yttria-based nano-sized powders: A new class of fractal materials obtained by combustion synthesis. J. Mater. Res. 15, 586 (2000).
20. A.M. Hecht, E. Geissler, and F. Horkay: Structure of silica-filled poly (dimethyl siloxane) gels and solutions. Phys. Rev. E 59, 1976 (1999).
21. 4 spinel from micyoemulsion and CVD techniques. J. Appl. Crystallogr. 33, 507 (2000).
22. G. Beaucage, H.K. Kammler, and S.E. Pratsinis: Particle size distribution from small-angle scattering using global scattering functions. J. Appl. Crystallogr. 37, 523 (2004).
23. G. Beaucage: Determination of branch fraction and minimum dimension of mass-fractal aggregates. Phys. Rev. E 70, 031401 (2004).
24. J. Hyeon-Lee, G. Beaucage, S.E. Pratsinis, and S. Vemury: Fractal analysis of flame-synthesized nanostructured silica and titania powders using small-angle x-ray scattering. Langmuir 14, 5751 (1998).
25. T. Koga, M. Takenaka, K. Aizawa, M. Nakamura, and T. Hashimoto: Structure factors of dispersible units of carbon black filler in rubbers. Langmuir 21, 11409 (2005).
26. H.K. Kammler, G. Beaucage, R. Mueller, and S.E. Pratsinis: Structure of flame-made silica nanoparticles by ultra-small-angle x-ray scattering. Langmuir 20, 1915 (2004).
27. O. Glatter and O, Kratky: Small Angle X-ray, Scattering (Academic Press, London, UK, 1982).
28. G. Beaucage: Approximations leading to a unified exponential/power-law approach to small-angle scattering. J. Appl. Crystallogr. 28, 717 (1995).
29. A. Guinier: X-ray Diffraction (W.H. Freeman and Company, San Francisco, CA, 1963).
30. T. Freltoft, J.K. Kjems, and S.K. Sinha: Power-law correlations and finite-size effects in silica particle aggregates studied by small-angle neutron scattering. Phys. Rev. B 33, 269 (1986).
31. I. Markovic and R.H. Ottewill: Small angle neutron scattering studies on aqueous dispersions of calcium carbonate, Part 2. Determination of the form factor for concentric spheres. Colloid Polym. Sci. 264, 65 (1986).
32. M. Kotlarchyk and S.H. Chen: Analysis of small angle neutron scattering spectra from polydisperse interacting colloids. J. Chem. Phys. 79, 2461 (1983).
33. J.S. Pedersen: Analysis of small-angle scattering data from colloids and polymer solutions: Modeling and least-squares fitting. Adv. Colloid Interface Sci. 70, 171 (1997).
34. J.A. Potton, G.J. Daniell, and B.D. Rainford: Particle size distributions from SANS data using the maximum entropy method. J. Appl. Crystallogr. 21, 663 (1988).
35. P.R. Jermian, G.G. Long, F. Lofaj, and S.M. Wiederhorn: Anomalous ultra-small-angle x-ray scattering from evolving microstructures during tensile creep, in Applications of Synchrotron Radiation Techniques to Materials Science V, edited by S.R. Stock. S.M. Mini, and D.L. Perry, (Mater. Res. Soc. Symp. Proc. 590, Pittsburgh, PA, 21000), p. 131.
36. L.B. Kiss, J. Soderlund, G.A. Niklasson, and C.G. Granqvist: The real origin of log-normal size distributions of nanoparticles in vapor growth processes. Nanostruct. Mater. 12, 327 (1999).
37. T.P. Rieker and P.F. Hubbard: The university of New Mexico/Sandia National Laboratories small-angle scattering laboratory. Rev. Sci. Instrum. 69, 3504 (1998).
38. J.A. Lake: An iterative method of slit-correcting small angle x-ray data. Acta Crystallogr. 23, 191 (1967).
39. P.A. Seeger and R.P. Hjelm: Small-angle neutron scattering at pulsed spaliation sources. J. Appl. Crystallogr. 24, 467 (1991).
40. R.P. Hjelm: The resolution of TOF low-Q diffractometers: Instrumental, data acquisition and reduction factors. J. Appl. Crystallogr. 21, 618 (1988).
41. S. Mazumder, A. Sequeira, S.K. Roy, and A.R. Biswas: Multiple small-angle scattering: An experimental investigation. J. Appl. Crystallogr. 26, 357 (1993).
42. A. Guinier and G. Fournet: Small-Angle Scattering of X-rays (John Wiley and Sons, New York, 1955).