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34447541235
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note
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-1): 1587m, 1533s, 1421s, 1349w, 1286w,1205w, 1105w, 1026w, 792m, 703m, 687m.
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11
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34447535606
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note
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2 with anisotropic parameters for all non-hydrogen atoms. The hydrogen atoms in the structure were placed geometrically and included in the structure factor calculation in the riding motion approximation. All calculations were performed with the use of the SAINT [13] and SHELXTL-97 [14] program packages.
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34447541346
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G.M. Sheldrick, SADABS, 1997, Bruker AXS Inc., Madison, WI-53719, USA.
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13
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34447533376
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SMART V5.051 and SAINT V5.00, Area detector control and integration software, 1998, Bruker AXS Inc., Madison, WI-53719, USA.
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14
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34447554955
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G.M. Sheldrick, SHELXTL-97 V5.10, 1997, Bruker AXS Inc., Madison, WI-53719, USA.
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34447569735
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note
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2O recovered the starting material only.
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34447554954
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note
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2 with anisotropic parameters for all non-hydrogen atoms. The hydrogen atoms in the structure were placed geometrically and included in the structure factor calculation in the riding motion approximation. All calculations were performed with the use of the SAINT [13] and SHELXTL-97 [14] program packages.
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