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X-ray crystal structure analysis of 6.2A: A single crystal was mounted on top of a glass capillary. Diffraction data were collected at 150 K with a Siemens P4RA four-cyrcle diffractometer utilizing monochromated Mo-Kα, radiation. The data were corrected for absorption (ψ-scan method) as well as for Lorentz and polarisation effects. The structure was solved by direct methods and refined by full-matrix least-squares methods based on F2 with anisotropic displacement parameters for all non-hydrogen atoms using the SHELX-97* program suite. Hydrogen atoms were fixed on ideal positions and refined with a common isotropic temperature factor. The final refinement converged to R1, 0.0431 for 3201 data with Fo > 4σ(F o) and wR2, 0.1229 for all 4099 data and 263 parameters. CCDC-644405 contains the supplementary crystallographic data for this paper. These da
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2 = 0.1229 for all 4099 data and 263 parameters. CCDC-644405 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.
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