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Crystal data for NOCbl. Empirical formula: C62H 89N14O15PCo: Mr, 1359 g mol-1; orthorhombic; space group P212 121: a, 15.930, b, 21.390, c, 24.066 Å; V, 8200.3(1) Å3; Z, 4; absorption coefficient, 0.29 mm-1; F(000, 3912; limiting indices: -18 ≤ h ≤ 18, 26 ≤ k ≤ 26, 29 ≤ l ≤ 29; reflections collected/unique: 39700/17159; Rmerge and Rsym: 0.035, 0.041; refinement method: full-matrix least squares on F2; data/ restraints/parameters: 15872/0/1036; GOF on F2: 0.975; R factors (I > 4σI, R1= 0.0964, wR2, 0.2786; R factor all data, R1, 0.1061; largest difference peak and hole: +0.53 and -0.46 e Å-3. CCDC-6
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