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Volumn 46, Issue 27, 2007, Pages 5140-5143

Nitroxylcob(III)alamin: Synthesis and X-ray structural characterization

Author keywords

Cobalamins; N ligands; Nitrogen oxides; Structure elucidation; Vitamin B 12

Indexed keywords

COBALAMINS; STRUCTURE ELUCIDATION; X RAY STRUCTURAL CHARACTERIZATION;

EID: 34447326743     PISSN: 14337851     EISSN: None     Source Type: Journal    
DOI: 10.1002/anie.200701131     Document Type: Article
Times cited : (42)

References (29)
  • 2
    • 34447340424 scopus 로고    scopus 로고
    • .NO.
    • .NO.
  • 18
    • 34447314363 scopus 로고    scopus 로고
    • Crystal data for NOCbl. Empirical formula: C62H 89N14O15PCo: Mr, 1359 g mol-1; orthorhombic; space group P212 121: a, 15.930, b, 21.390, c, 24.066 Å; V, 8200.3(1) Å3; Z, 4; absorption coefficient, 0.29 mm-1; F(000, 3912; limiting indices: -18 ≤ h ≤ 18, 26 ≤ k ≤ 26, 29 ≤ l ≤ 29; reflections collected/unique: 39700/17159; Rmerge and Rsym: 0.035, 0.041; refinement method: full-matrix least squares on F2; data/ restraints/parameters: 15872/0/1036; GOF on F2: 0.975; R factors (I > 4σI, R1= 0.0964, wR2, 0.2786; R factor all data, R1, 0.1061; largest difference peak and hole: +0.53 and -0.46 e Å-3. CCDC-6
    • -3. CCDC-642210 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/ data_request/cif.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.