Use of liquid chromatography-atmospheric pressure chemical ionization-ion trap mass spectrometry for identification of oleanolic acid and ursolic acid in Anoectochilus roxburghii (wall.) Lindl

Journal of Mass Spectrometry

Volumn 42, Issue 7, 2007, Pages 910-917

  Huang, Liying ^a,b   Chen, Tianwen ^a,c   Ye, Zhao ^c   Chen, Guonan ^a  

^a BEIJING UNIVERSITY OF POSTS AND TELECOMMUNICATIONS   (China)

^b FUJIAN MEDICAL UNIVERSITY   (China)

^c FUZHOU UNIVERSITY   (China)

Author keywords

Anoectochilus roxburghii; Liquid chromatography atmospheric pressure chemical ionization ion trap mass spectrometry; Oleanolic acid; Supercritical fluid extraction; Ursolic acid

Indexed keywords

ANOECTOCHILUS ROXBURGHII; CHEMICAL IONIZATION; OLEANOLIC ACID; URSOLIC ACID;

ATMOSPHERIC PRESSURE; BIOACTIVITY; IONIZATION; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; PLANTS (BOTANY); SUPERCRITICAL FLUID EXTRACTION;

ORGANIC ACIDS;

ACETIC ACID; ALCOHOL; CARBON DIOXIDE; METHANOL; OLEANOLIC ACID; URSOLIC ACID; WATER;

ANOECTOCHILUS ROXBURGHII; ARTICLE; ATMOSPHERIC PRESSURE; CONTROLLED STUDY; DRUG IDENTIFICATION; DRUG ISOLATION; DRUG STRUCTURE; FLOW RATE; ION MONITORING; LIQUID CHROMATOGRAPHY; MASS SPECTROMETER; MASS SPECTROMETRY; NONHUMAN; ORCHIDACEAE; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; SEPARATION TECHNIQUE; SUPERCRITICAL FLUID EXTRACTION;

CARBON DIOXIDE; CHROMATOGRAPHY, LIQUID; CHROMATOGRAPHY, SUPERCRITICAL FLUID; MASS SPECTROMETRY; OLEANOLIC ACID; PLANTS; REPRODUCIBILITY OF RESULTS; SOLVENTS; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; TRITERPENES;

ANOECTOCHILUS ROXBURGHII;

EID: 34447309563     PISSN: 10765174     EISSN: 10969888     Source Type: Journal    
DOI: 10.1002/jms.1228     Document Type: Article

References (23)

1. He C-N, Wang C-L, Guo S-X, Xiao P-G. A review of research on chemical composition and pharmacological activities of anoectochilus roxburghii plant. Chinese Pharmaceutical Journal 2004; 39: 81.
2. Wen-yan CAI, Hua-shan XIAO, Xiu-zhen FAN. A review of research on anoectochilus roxburghii. Subtropical Plant Science 2003; 32: 68.
3. Lin J-M, Lin C-C, Chiu H-F, Yang J-J, Lee S-GT. Evaluation of the anti-inflammatory and liver-protective effects of anoectochilus formosanus ganoderma lucidum and gynostemma pentaphyllum in rats. American Journal of Chinese Medicine 1993; 21: 59.
4. Shyur L-F, Chenb C-H, Lo C-P, Wang S-Y, Kang P-L, Sun S-J, Chang CA, Tzeng C-M, Yang N-S. Induction of apoptosis in mcf-7 human breast cancer cells by phytochemicalsfrom Anoectochilus formosanus. Journal of Biomedical Science 2004; 11: 928.
5. Lin JM, Lin CC, Chiu HF. Evaluation of the anti-inflammatory and liver-protective effects of anoectochilus formosanus ganoderma lucidum and gynostemma pentaphyllum in rats. American Journal of Chinese Medicine 1993; 21: 59.
6. Lin CC, Huang PC, Lin JM. Antioxidant and hepatoprotective effects of anoectochilus formosanus and gynostemma pentaphyllum. American Journal of Chinese Medicine 2000; 28: 87.
7. Shih CC, Wu YW, Lin WC. Scavenging of reactive oxygen species and inhibition of the oxidation of low density lipoprotein by the aqueous extract of anoectochilus formosanus. American Journal of Chinese Medicine 2002; 31: 25.
8. Xiao-Ming DU, Ning-Yi SUN, Takashi T, Mohri A, Sugiura M, Yoshizawa T, Irino N, Hayashi J, Shoyama Y. Higher yielding isolation of kinsenoside in anoectochilus and its antihyperliposis effect. Biological and Pharmaceutical Bulletin 2001; 24: 65.
9. Du X-M, Ning-Yi I, Irino N, Shoyama Y. Glycoside constituents from anoectochilus formosanus. Chemical and Pharmaceutical Sciences 2000; 48: 1803.
10. Ito A, Kasai K, Yanasaki K, Sugimoto H. Aliphatic and aromatic glucoside from, anoectochilus koshunensis. Phytochemistry 1993; 33: 1133.
11. Ito A, Yasumoto K, Kasai R, Yamasaki K. A sterol with an unusual side chain from anoectochilus koshunensis. Phytochemistry 1994; 36: 1465.
12. Song M, Hang T-J, Wang Y, Jiang L, Wu X-L, Zhang Z, Shen J, Zhang Y. Determination of oleanolic acid in human plasma and study of its pharmacokinetics in Chinese healthy male volunteers by HPLC tandem mass spectrometry. Journal of Pharmaceutical and Biomedical Analysis 2006; 40: 190.
13. Zhi-jie MA, Hong-you HU. A review of research on the local medicinal herb "jin-xian-lian". Subtropical Plant Science 2002; 31: 27.
14. Junxan Z, Huilan H, Guixian Q, Dong L. Determination of oleanolic acid in hou yan ning oral administration by thin layer scanning method. Academic Journal Guangdong College of Pharmacy 2000; 16: 204.
15. Huali Y, Luhua Z, Danni Z, Li D. Determination of oleanol ic acid and ursolic acid in spica prunellae by derivative GC method. Zhongguo Zhongyao Zazhi 2001; 24: 744.
16. Chen JH, Xia ZH, Tan RX. High-performance liquid chromatographic analysis of bioactive triterpenes in perilla frutescens. Journal of Pharmaceutical and Biomedical Analysis 2003; 32: 1175.
17. Claudea B, Morina P, Lafossea M, Andreb P. Evaluation of apparent formation constants of pentacyclic triterpene acids complexes with derivatize and cyclodextrins by reversed phase liquid chromatography. Journal of Chromatography A 2004; 1049: 37.
18. Hu Y, Wang Y, Luo G, Wei W. Determination of oleanolic acid in ligustrum by capillary electrophoresis. Analytical Letters 2000; 33: 357.
19. Qi S, Ding L, Tian K, Chen X, Hua Z. Novel and simple nonaqueous capillary electrophoresis separation and determination bioactive triterpenes in Chinese herbs. Journal of Pharmaceutical and Biomedical Analysis 2006; 40: 35.
20. Careri M, Furlattini L, Mangia A, Musci M, Anklam E, Theobald A, Von Holst C. Supercritical fluid extraction for liquid chromatographic determination of carotenoids in spirulina pacifica algae a chemometric approach. Journal of Chromatography A 2001; 912: 61.
21. Lin M-C, Tsai M-J, Wen K-C. Supercritical fluid extraction of flavonoids from Scutellariae radix. Journal of Chromatography A 1999; 830: 387.
22. Pamme N, Steinbach K, Ensinger WJ, Schmidt TC. Analysis of polynitrophenols and hexyl by liquid chromatography mass spectrometry using atmospheric pressure ionisation methods and a volatile ion-pairing reagent. Journal of Chromatography A 2001; 943: 47.
23. Michielin EMZ, Bresciani LFV, Danielskic L, Yunes RA, Ferreira SRS. Composition profile of horsetail (Equisetum gigantenum L.) oleoresin:comparing SFE and organic solvents extraction. Journal of Supercritical Fluids 2005; 33: 131.