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This is the method reported for the synthesis of 3 reference [15, Since products were characterized only by elemental analysis in reference [15, oxygen migration might have gone unnoticed by the authors
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This is the method reported for the synthesis of 3 (reference [15]). Since products were characterized only by elemental analysis in reference [15], oxygen migration might have gone unnoticed by the authors.
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18
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0032547296
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Starting N-alkyl sulfinamides were prepared from the thiosulfinate reported by Ellman and co-workers and the corresponding lithium amide; see: D. A. Cogan, G. Liu, K. Kim, B. J. Backes, J. A. Ellman, J. Am. Chem. Soc. 1998, 120, 8011.
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Starting N-alkyl sulfinamides were prepared from the thiosulfinate reported by Ellman and co-workers and the corresponding lithium amide; see: D. A. Cogan, G. Liu, K. Kim, B. J. Backes, J. A. Ellman, J. Am. Chem. Soc. 1998, 120, 8011.
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The highest optical purity described for this compound was 80% ee; see: A. M. Hay, W. J. Kerr, G. G. Kirk, D. Middlemiss, Organometallics 1995, 14, 4986.
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The highest optical purity described for this compound was 80% ee; see: A. M. Hay, W. J. Kerr, G. G. Kirk, D. Middlemiss, Organometallics 1995, 14, 4986.
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