Indirect covariance NMR spectroscopy of through-bond homo-nuclear correlations for quadrupolar nuclei in solids under high-resolution

Solid State Nuclear Magnetic Resonance

Volumn 31, Issue 4, 2007, Pages 163-168

  Hu, Bingwen ^a   Amoureux, Jean Paul ^a   Trebosc, Julien ^a  

^a UNIV LILLE   (France)

Author keywords

GEN2D; H HSQC experiment; Indirect covariance; J coupling; MQ HETCOR; MQ HOMCOR; ST HETCOR; ST HOMCOR

Indexed keywords

CORRELATION METHODS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SPECTROMETERS;

H-HSQC EXPERIMENTS; INDIRECT-COVARIANCE; MEDIUM-FIELD SPECTROMETERS; MQ-HETCOR; MQ-HOMCOR;

CHEMICAL BONDS;

ARTICLE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; NUCLEAR PHYSICS;

MAGNETIC RESONANCE SPECTROSCOPY; NUCLEAR PHYSICS;

EID: 34347392474     PISSN: 09262040     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.ssnmr.2007.03.002     Document Type: Article

References (32)

1. Ernst R.R., Bodenhausen G., and Wokaun A. Principles of Nuclear Magnetic Resonance in One or Two dimensions (1987), Clarendon Press, Oxford
2. Lesage A., Bardet M., and Emsley L. Through-bond carbon-carbon connectivities in disordered solids by NMR. J. Am. Chem. Soc. 121 (1999) 10987-10993
3. Fayon F., Le Saout G., Emsley L., and Massiot D. Through-bond phosphorus-phosphorus connectivities in crystalline and disordered phosphates by solid-state NMR. Chem. Commun. (2005) 1702-1703
4. Deschamps M., Fayon F., Montouillout V., and Massiot D. Through-bond homonuclear correlation experiments in solid-state NMR applied to quadrupolar nuclei in Al-O-P-O-Al chains. Chem. Commun. (2006) 1924-1925
5. 27Al networks. J. Magn. Reson. 184 (2006) 15-19
6. Kundla E., Samoson A., and Lippmaa E. High-resolution NMR of quadrupolar nuclei in rotating solids. Chem. Phys. Lett. 83 (1981) 229-232
7. Frydman L., and Harwood J.S. Isotropic spectra of half-integer quadrupolar spins from bidimensional MAS NMR. J. Am. Chem. Soc. 117 (1995) 5367-5368
8. Gan Z. Isotropic spectra of half-integer quadrupolar nuclei using satellite transitions and MAS. J. Am. Chem. Soc. 122 (2000) 3242-3243
9. Noda I. Two-dimensional infrared spectroscopy. J. Am. Chem. Soc. 111 (1989) 8116-8118
10. Noda I. Generalized 2-dimensional correlation method applicable to infrared, Raman, and other types of spectroscopy. Appl. Spectrosc. 47 (1993) 1329-1336
11. Noda I. Determination of two-dimensional correlation spectra using the Hilbert transform. Appl. Spectrosc. 54 (2000) 994-999
12. Noda I., Dowrey A.E., Marcott C., Story G.M., and Ozaki Y. Generalized two-dimensional correlation spectroscopy. Appl. Spectrosc. 54 (2000) 236A-248A
13. Eads C.D., and Noda I. Generalized correlation NMR spectroscopy. J. Am. Chem. Soc. 124 (2002) 1111-1118
14. Brüschweiler R., and Zhang F. Covariance NMR spectroscopy. J. Chem. Phys. 120 (2004) 5253-5260
15. Hu B.W., Zhou P., Noda I., and Zhao G.Z. An NMR approach applicable to biomolecular structure characterization. Anal. Chem. 77 (2005) 7534-7538
16. Zhang F., and Brüschweiler R. Indirect covariance NMR spectroscopy. J. Am. Chem. Soc. 126 (2004) 13180-13181
17. Blinov K.A., Larin N.I., Kvasha M.P., Moser A., Williams A.J., and Martin G.E. Analysis and elimination of artifacts in indirect covariance NMR spectra via unsymmetrical processing. Magn. Reson. Chem. 43 (2005) 999-1007
18. Wiench J.W., and Pruski M. Probing through-bond connectivities with MQMAS NMR. Solid. State NMR 26 (2004) 51-55
19. Amoureux J.P., Trebosc J., Wiench J., and Pruski M. HMQC and refocused-INEPT experiments involving half-integer quadrupolar nuclei in solids. J. Magn. Reson. 184 (2006) 1-14
20. Wiench J.W., Tricot G., Delevoye L., Trebosc J., Frye J., Montagne L., Amoureux J.P., and Pruski M. SPAM-MQ-HETCOR: an improved method for hetero-nuclear correlation spectroscopy between quadrupolar and spin-1/2 nuclei in solid-state NMR. Phys. Chem. Chem. Phys. 8 (2006) 144-150
21. 15N NMR: polarization transfer using the INEPT pulse sequence. J. Am. Chem. Soc. 102 (1980) 428-429
22. Burum D.P., and Ernst R.R. Net polarization transfer via a J-ordered state for signal enhancement of low-sensitivity nuclei. J. Magn. Reson. 39 (1980) 163-168
23. Bennet A.E., Rienstra C.M., Auger M., Lakshmi K.V., and griffin R.G. Hetero-nuclear decoupling in rotating solids. J. Chem. Phys. 103 (1995) 6951-6958
24. Delevoye L., Trebosc J., Gan Z., Montagne L., and Amoureux J.P. Resolution enhancement using a new multiple-pulse decoupling sequence for quadrupolar nuclei. J. Magn. Reson. 186 (2007) 94-99
25. Broach R.W., Wilson S.T., and Kirchner R.M. Micropor. Mesopor. Mater. 57 (2003) 211
26. 27Al MQMAS and STMAS NMR spectroscopy. J. Am. Chem. Soc. 128 (2006) 8054-8062
27. Ashbrook S.E., Antonijevic S., Berry A.J., and Wimperis S. Motional broadening: an important distinction between multiple-quantum and satellite-transition MAS NMR of quadrupolar nuclei. Chem. Phys. Lett. 364 (2002) 634-642
28. Trebosc J., Amoureux J.P., and Gan Z. Comparison of high-resolution solid-state NMR MQMAS and STMAS methods for half-integer quadrupolar nuclei. Solid. State NMR 30 (2006) 182-190
29. 4-14. Enhanced resolution and information by MQMAS. Micropor. Mater. 6 (1996) 331-340
30. 4-14. Solid. State NMR 9 (1997) 97-106
31. 31P MQ-HETCOR NMR. Solid. State NMR 22 (2002) 501-512
32. Fayon F., King I.J., Harris R.K., Evans J.S.O., and Massiot D. Application of the through-bond correlation NMR experiment to the characterization of crystalline and disordered phosphates. C.R. Chimie 7 (2004) 351-361