HMQC and refocused-INEPT experiments involving half-integer quadrupolar nuclei in solids

Journal of Magnetic Resonance

Volumn 184, Issue 1, 2007, Pages 1-14

  Amoureux, J P ^a   Trebosc, J ^a   Wiench, J ^b   Pruski, M ^b  

^a UNITÉ DE CATALYSE ET DE CHIMIE DU SOLIDE   (France)

^b IOWA STATE UNIVERSITY   (United States)

Author keywords

HMQC; J coupling; MAS; MQMAS; Quadrupolar nuclei; R INEPT; Solid state NMR; STMAS

Indexed keywords

COHERENT LIGHT; LIGHT TRANSMISSION; OPTICAL RESOLVING POWER; QUANTUM THEORY; SOLID STATE DEVICES;

HMQC; J COUPLING; MAS; MQMAS; QUADRUPOLAR NUCLEI; R-INEPT; SOLID STATE NMR; STMAS;

NUCLEAR MAGNETIC RESONANCE;

ALUMINUM DERIVATIVE; ALUMINUM PHOSPHATE; PHOSPHATE;

ALGORITHM; ARTICLE; CHEMICAL MODEL; CHEMICAL STRUCTURE; CHEMISTRY; COMPUTER SIMULATION; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SPIN LABELING;

ALGORITHMS; ALUMINUM COMPOUNDS; COMPUTER SIMULATION; MAGNETIC RESONANCE SPECTROSCOPY; MODELS, CHEMICAL; MODELS, MOLECULAR; PHOSPHATES; SPIN LABELS;

EID: 33846018074     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2006.09.009     Document Type: Article

References (73)

1. Ernst R.R., Bodenhausen G., and Wokaun A. Principles of Nuclear Magnetic Resonance in One and Two Dimensions (1991), Clarendon Press, Oxford
2. Terao T., Miura H., and Saika A. High-resolution J-resolved NMR spectra of dilute spins in solids. J. Chem. Phys. 75 (1981) 1573-1574
3. Zilm K.W., and Grant D.M. High-resolution NMR spectra with J couplings in solids. J. Magn. Reson. 48 (1982) 524-526
4. 207Pb NMR study of organotin and organolead chalcogenides: observation of J-coupling in solids. Magn. Reson. Chem. 27 (1989) 81-87
5. Chu P.J., Lunsford J.H., and Zalewski D.J. Structural information from the J-coupled multiplet of a (trimethylphosphine)trichloroaluminum coordination complex on zeolite Y. J. Magn. Reson. 87 (1990) 68-79
6. Fyfe C.A., Wong-Moon K.C., Huang Y., and Grondey H. INEPT experiments in solid-state NMR. J. Am. Chem. Soc. 117 (1995) 10397-10398
7. Kao H.-M., and Grey C.P. INEPT experiments involving quadrupolar nuclei in solids. J. Magn. Reson. 133 (1998) 313-323
8. 27Al J-coupling constant for trimethylphosphine bound to the lewis acid site of zeolite HY. J. Am. Chem. Soc. 119 (1997) 627-628
9. Brown S.P., Perez-Torralba M., Sanz D., Claramunt R.M., and Emsley L. Determining hydrogen-bond strengths in the solid state by NMR. The quantitative measurement of homonuclear J couplings. Chem. Commun. (2002) 1852-1853
10. Trebosc J., Amoureux J.P., Wiench J.W., and Pruski M. Simultaneous frequency-selective solid-state NMR analysis of internuclear distances and through-bond connectivities in the presence of quadrupolar nuclei. Chem. Phys. Lett. 374 (2003) 432-438
11. Trebosc J., Amoureux J.P., Delevoye L., Wiench J.W., and Pruski M. Frequency-selective measurement of heteronuclear scalar couplings in solid-state NMR. Solid State Sci. 6 (2004) 1089-1095
12. 13C spectra by using J-resolved NMR spectroscopy in solids. J. Am. Chem. Soc. 104 (1982) 5228-5229
13. 13C cross polarization/magic angle spinning NMR of solids. J. Magn. Reson. 79 (1988) 554-560
14. Tekely P., Brondeau J., Retournard A., and Canet D. Partial editing in heteronuclear J-resolved solid-state NMR spectroscopy. Magn. Reson. Chem. 27 (1989) 696-698
15. Sakellariou D., Lesage A., and Emsley L. Spectral editing in solid-state NMR using scalar multiple quantum filters. J. Magn. Reson. 151 (2001) 40-47
16. Early T.A., John B.K., and Johnson L.F. Observation of homonuclear double-quantum correlations in plastic crystals using cross polarization and magic angle spinning. J. Magn. Reson. 75 (1987) 134-138
17. 29Si INADEQUATE and COSY type experiments. J. Chem. Soc., Chem. Commun. (1988) 102-103
18. 29Si NMR investigations of three-dimensional lattice connectivities in zeolite structures. J. Am. Chem. Soc. 112 (1990) 3264-3270
19. Lesage A., Auger C., Caldarelli S., and Emsley L. Determination of through-bond carbon-carbon connectivities in solid-state NMR using the INADEQUATE Experiment. J. Am. Chem. Soc. 119 (1997) 7867-7868
20. 15N J coupling. J. Am. Chem. Soc. 124 (2002) 1152-1153
21. Fayon F., Roiland C., Emsley L., and Massiot D. Triple-quantum correlation NMR experiments in solids using J-couplings. J. Magn. Reson. 179 (2006) 49-57
22. 29Si magic angle spinning NMR investigation of the silicate lattice of zeolite ZSM-39 (Dodecasil 3C). J. Am. Chem. Soc. 111 (1989) 7702-7707
23. Baldus M., and Meier B.H. Total correlation spectroscopy in the solid state. The use of scalar couplings to determine the through-bond connectivity. J. Magn. Reson. A 121 (1996) 65-69
24. Caravatti P., Bodenhausen G., and Ernst R.R. Heteronuclear solid-state correlation spectroscopy. Chem. Phys. Lett. 89 (1982) 363-367
25. Burum D.P., and Bielecki A. An improved experiment for heteronuclear-correlation 2D NMR in solids. J. Magn. Reson. 94 (1991) 645-652
26. 13C NMR heteronuclear dipolar-correlation spectroscopy of solids with frequency-switched Lee-Goldburg homonuclear decoupling. J. Magn. Reson. 124 (1997) 516-519
27. Hing A.W., Vega S., and Schaefer J. J. Magn. Reson. 96 (1992) 205-209
28. Amoureux J.P., and Pruski M. In: Grant D.M., and Harris R.K. (Eds). Advances in MQMAS NMR 9 (2002), Wiley, London 226-251
29. Brown S.P., and Spiess H.W. Advanced solid-state NMR methods for the elucidation of structure and dynamics of molecular, macromolecular, and supramolecular systems. Chem. Rev. 101 (2001) 4125-4155
30. Trebosc J., Wiench J.W., Huh S., Lin V.S.Y., and Pruski M. Studies of organically functionalized mesoporous silicas using heteronuclear solid-state correlation NMR spectroscopy under fast magic angle spinning. J. Am. Chem. Soc. 127 (2005) 7587-7593
31. Opella S.J. Multiple-resonance multi-dimensional solid-state NMR of proteins. Encyclopedia NMR 9 (2002) 427-436
32. Miura H., Terao T., and Saika A. Heteronuclear two-dimensional J spectroscopy in rigid solids. J. Magn. Reson. 68 (1986) 593-596
33. Anderson M.W., and Klinowski J. Monitoring organic products of catalytic reactions on zeolites by two-dimensional J-resolved solid-state NMR. Chem. Phys. Lett. 172 (1990) 275-278
34. 4-14. Solid State Nucl. Magn. Reson. 9 (1997) 97-106
35. Lesage A., Sakellariou D., Steuernagel S., and Emsley L. Carbon-proton chemical shift correlation in solid-state NMR by through-bond multiple-quantum spectroscopy. J. Am. Chem. Soc. 120 (1998) 13194-13201
36. Massiot D., Fayon F., Alonso B., Trebosc J., and Amoureux J.-P. Chemical bonding differences evidenced from J-coupling in solid state NMR experiments involving quadrupolar nuclei. J. Magn. Reson. 164 (2003) 160-164
37. Amoureux J.P., Trebosc J., Wiench J.W., Massiot D., and Pruski M. Frequency selective solid state NMR measurement of J couplings between spin-1/2 and quadrupolar nuclei. Solid State Nucl. Magn. Reson. 27 (2005) 228-232
38. Iuga D., Morais C., Gan Z., Neuville D.R., Cormier L., and Massiot D. NMR heteronuclear correlation between quadrupolar nuclei in solids. J. Am. Chem. Soc. 127 (2005) 11540-11541
39. Deschamps M., Fayon F., Montouillout V., and Massiot D. Trough-bond homonuclear correlation experiments in solid-state NMR applied to quadrupolar nuclei in Al-O-P-O-Al chains. Chem. Comm (2006) 1924-1925
40. Wiench J.W., and Pruski M. Probing through bond connectivities with MQMAS NMR. Solid State Nucl. Magn. Reson. 26 (2004) 51-55
41. Frydman L., and Harwood J.S. Isotropic spectra of half-integer quadrupolar spins from bidimensional magic-angle spinning NMR. J. Am. Chem. Soc. 117 (1995) 5367-5368
42. Vega A.J. MAS NMR spin locking of half-integer quadrupolar nuclei. J. Magn. Reson. 96 (1992) 50-68
43. Vega A.J. CP/MAS of quadrupolar S = 3/2 nuclei. Solid State Nucl. Magn. Reson. 1 (1992) 17-32
44. Amoureux J.P., and Pruski M. Theoretical and experimental assessment of single and multiple-quantum cross-polarization in solid-state NMR. Mol. Phys. 100 (2002) 1595-1613
45. Morris G.A., and Freeman R. Enhancement of nuclear magnetic resonance signals by polarization transfer. J. Am. Chem. Soc. 101 (1979) 760-762
46. Gan Z. Isotropic NMR spectra of half-integer quadrupolar nuclei using satellite transitions and magic-angle spinning. J. Am. Chem. Soc. 122 (2000) 3242-3243
47. 15N NMR: polarization transfer using the INEPT pulse sequence. J. Am. Chem. Soc. 102 (1980) 428-429
48. Burum D.P., and Ernst R.R. Net polarization transfer via a J-ordered state for signal enhancement of low-sensitivity nuclei. J. Magn. Reson. 39 (1980) 163-168
49. Pegg D.T., Doddrell D.M., Brooks W.M., and Bendall M.R. Proton polarization transfer enhancement for a nucleus with arbitrary spin quantum number from n scalar coupled protons for arbitrary preparation times. J. Magn. Reson. 44 (1981) 32-40
50. Sørensen O.W., and Ernst R.R. Elimination of spectral distortion in polarization transfer experiments. Improvements and comparison of techniques. J. Magn. Reson. 51 (1983) 477-489
51. Doddrell D.M., Pegg D.T., and Bendall M.R. Distortionless enhancement of NMR signals by polarization transfer. J. Magn. Reson. 48 (1982) 323-327
52. 15N NMR by enhanced heteronuclear spectroscopy. Chem. Phys. Lett. 69 (1980) 185-189
53. 15N and proton chemical shifts in natural-abundance samples via multiple quantum coherence. J. Am. Chem. Soc. 105 (1983) 7188-7190
54. Pegg D.T., and Bendall M.R. Coupled polarization transfer spectra for higher-spin nuclei. J. Magn. Reson. 58 (1984) 14-26
55. Burum D.P. Heteronuclear correlated 2D NMR spectroscopy of spins greater than 1/2. Application to decaborane. J. Magn. Reson. 59 (1984) 430-436
56. Zwahlen C., Legault P., Vincent S.J.F., Greenblatt J., Konrat R., and Kay L.E. Methods for measurement of intermolecular NOEs by multinuclear NMR spectroscopy: application to a bacteriophage lN-peptide/boxB RNA complex. J. Am. Chem. Soc. 119 (1997) 6711-6721
57. Yao Z., Kwak H.T., Sakellariou D., Emsley L., and Grandinetti P.J. Sensitivity enhancement of the central transition NMR signal of quadrupolar nuclei under magic-angle spinning. Chem. Phys. Lett. 327 (2000) 85-90
58. Kwak H.T., Prasad S., Yao Z., Grandinetti P.J., Sachleben J.R., and Emsley L. Enhanced sensitivity in RIACT/MQ-MAS NMR experiments using rotor assisted population transfer. J. Magn. Reson. 150 (2001) 71-80
59. Madhu P.K., Goldbourt A., Frydman L., and Vega S. Sensitivity enhancement of the MQMAS NMR experiment by fast amplitude modulation of the pulses. Chem. Phys. Lett. 307 (1999) 41-47
60. Kentgens A.P.M., and Verhagen R. Advantages of double frequency sweeps in static, MAS and MQMAS NMR of spin I = 3/2 nuclei. Chem. Phys. Lett. 300 (1999) 435-443
61. Siegel R., Nakashima T.T., and Wasylishen R.E. Signal enhancement of NMR spectra of half-integer quadrupolar nuclei in solids using hyperbolic secant pulses. Chem. Phys. Lett. 388 (2004) 441-445
62. Vosegaard T., Larsen F.H., Jakobsen H.J., Ellis P.D., and Nielsen N.C. Sensitivity-enhanced multiple-quantum MAS NMR of half-integer quadrupolar nuclei. J. Am. Chem. Soc. 119 (1997) 9055-9056
63. Lefort R., Wiench J.W., Pruski M., and Amoureux J.P. Optimization of data acquisition and processing in Carr-Purcell-Meiboom-Gill multiple quantum magic angle spinning nuclear magnetic resonance. J. Chem. Phys. 116 (2002) 2493-2501
64. Goiffon A., Jumas J.C., Aurin M.M., and Philippot E. Structure studies of α-quartz type phases of MIIIXVO4 (MIII = Al, Ga and XV = P, As) at temperatures of 172, 293 and 373 K. J. Solid State Chem. 61 (1986) 384-396
65. Huguenard C., Taulelle F., and Gan Z. Optimizing STMAS. J. Magn. Reson. 156 (2002) 131-137
66. Amoureux J.P., Fernandez C., and Dumazy Y. A useful tool for the elaboration of new solid-state NMR experiments: PULSAR. J. Chim. Phys. 92 (1995) 1939-1942
67. Helliwell M., Kaucic V., Cheetham G.M.T., Harding M.M., Kariuki B.M., and Rizkallah P.J. Structure determination from small crystals of two aluminophosphates CrAPO-14 and SAPO-43. Acta Crystallogr. B49 (1993) 413-420
68. 4-14. Enhanced resolution and information by MQMAS. Micropor. Mat. 6 (1996) 331-340
69. 31P MQHETCOR NMR. Solid State Nucl. Magn. Reson. 22 (2002) 501-512
70. Gan Z., and Kwak H.-T. Enhancing MQMAS sensitivity using signals from multiple coherence transfer pathways. J. Magn. Reson. 168 (2004) 346-351
71. Wiench J.W., Tricot G., Delevoye L., Trebosc J., Frye J., Montagne L., Amoureux J.-P., and Pruski M. SPAM-MQMAS-HETCOR: an improved method for heteronuclear spectroscopy between quadrupolar and spin-1/2 nuclei in solid-state NMR. Phys. Chem. Chem. Phys. 8 (2000) 144-150
72. 19F coupling, and fluorine motion. J. Phys. Chem. A105 (2001) 760-768
73. Damodaran K., Wiench J.W., Cabral de Menezes S.M., Lam Y.L., Trebosc J., Amoureux J.-P., and Pruski M. Modification of H-ZSM-5 zeolites with phosphorus. 2. Interaction between phosphorus and aluminum studied by solid-state NMR spectroscopy. Micropor. Mesopor. Mater. xxx (2006) 297-306