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Angewandte Chemie - International Edition

Volumn 46, Issue 16, 2007, Pages 2895-2898

Preparation of molecular alumoxane hydrides, hydroxides, and hydrogensulfides

(5) González Gallardo, Sandra a Jancik, Vojtech a Cea Olivares, Raymundo a Toscano, Rubén A a Moya Cabrera, Mónica a

a UNIVERSIDAD NACIONAL AUTÓNOMA DE MÉXICO (Mexico)

Author keywords

Aluminum; Alumoxanes; Hydrides; Hydrogensulfides; Hydrolysis

Indexed keywords

CONFORMATIONS; HYDRIDES; HYDROGEN SULFIDE; SYNTHESIS (CHEMICAL);

ALUMINUM DIHYDRIDE; ALUMOXANE HYDROGENSULFIDE; HETEROMETALLIC COMPOUNDS;

MOLECULAR DYNAMICS;

EID: 34250846404 PISSN: 14337851 EISSN: None Source Type: Journal
DOI: 10.1002/anie.200605081 Document Type: Article

Times cited : (56)

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29
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- Crystal data for 3·toluene: C60H 76Al2N4OS2 (987.33, monoclinic, space group I2/a, a, 22.857(5, b, 8.707(2, c, 28.967(5) Å, β, 96.22(3)°, V, 5731(2) Å3, Z, 4, ρcalcd, 1-144 g cm -3, F(000, 2120, λ, 0.71073 Å, T, 173(2) K, μ(MoKα, 0.165 mm-1. Of the 14094 measured reflections, 5046 were independent (Rint, 0.0730, The final refinements converged at R1, 0.0599 for I > 2σI, wR2, 0.1650 for all data. The final difference Fourier synthesis gave a min/max residual electron density of -0.214/+0.389 e Å-3
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30
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- Crystal data for 4: C46H60Al 2N4O3 (770.94, monoclinic, space group P21/n, a, 11.248(3, b, 21.112(4, c, 18.346(3) Å, β, 93.23(3)°, V, 4350(2) Å3, Z, 4, ρcalcd, 1.177 g cm -3, F(000, 1656, λ, 0.71073 Å, T, 173(2) K, μ(MoKα, 0.110 mm-1. Of the 7990 measured reflections, 7990 were independent (Rint, 0.0478, The final refinements converged at R1= 0.0528 for I > 2σI, wR2, 0.1028 for all data. The final difference Fourier synthesis gave a min/max residual electron density of -0.302/+0.283 e Å-3
- -3.

31
- 34250799458
- Crystal data for 5: C46H60Al 2N4O0.25S2.75 (815.10, orthorhombic, space group Pna21, a, 20.794(3, b, 9.525(2, c, 23.442(4) Å, V, 4643(1) Å3, Z, 4, ρcalcd, 1.166 g cm -3, F(000, 1744, λ, 0.71073 Å, T, 173(2) K, μ(MOKα, 0.222 mm-1. Flack parameter was refined to 0.05(12, Of the 13 896 measured reflections, 6121 were independent (Rint, 0.0740, The final refinements converged at R1, 0.0614 for I > 2σI, wR2, 0.1299 for all data. The final difference Fourier synthesis gave a min/max residual electron density of -0.212/+0.276 e Å-3. Data for the structures of 1 and 3-5 were measured on a Bruker-APEX three-circle diffractometer. Intensit
- [9] The hydrogen atoms from the OH and SH groups were localized from the difference electron-density map and refined isotropically. The twin law for 4 was determined as a 180° rotation around the real axis [101]. CCDC-630404-630407 contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam. ac.uk/data_request/cif.

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* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.