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Volumn 46, Issue 13, 2007, Pages 2306-2309

Synthesis of calix[3]dipyrrins by a modified Lindsey protocol

Author keywords

Copper; Macrocyclic ligands; Nickel; Porphyrinoids; Synthetic methods

Indexed keywords

ALDEHYDES; COPPER; IONS; NICKEL; SYNTHESIS (CHEMICAL);

EID: 34250823602     PISSN: 14337851     EISSN: None     Source Type: Journal    
DOI: 10.1002/anie.200604882     Document Type: Article
Times cited : (20)

References (35)
  • 3
    • 0024562778 scopus 로고    scopus 로고
    • 3-EtOH cocatalyst was reported to be advantageous for the synthesis of sterically hindered porphyrins, see: J. S. Lindsey, R. W. Wanger, J. Org. Chem. 1989, 54, 828.
    • 3-EtOH cocatalyst was reported to be advantageous for the synthesis of sterically hindered porphyrins, see: J. S. Lindsey, R. W. Wanger, J. Org. Chem. 1989, 54, 828.
  • 5
  • 19
    • 33746216388 scopus 로고    scopus 로고
    • Angew. Chem. Int. Ed. 2006, 45, 3150.
    • (2006) Chem. Int. Ed , vol.45 , pp. 3150
    • Angew1
  • 21
    • 2142724735 scopus 로고    scopus 로고
    • For the chemistry of calix[n]pyrroles and calix[n] bipyrroles, see: a P. A. Gale, J. L. Sessler, V. Král, Chem. Commun. 1998, 1;
    • For the chemistry of calix[n]pyrroles and calix[n] bipyrroles, see: a) P. A. Gale, J. L. Sessler, V. Král, Chem. Commun. 1998, 1;
  • 23
  • 25
  • 29
    • 34250884195 scopus 로고    scopus 로고
    • Crystallographic data for 1: C81H58Cl 5N6Ni3O15, Mw, 1708.71, monoclinic, space group P21/c (no. 14, a, 11.4510(17, b, 20.120(3, c, 31.920(5) Å, α, 90, β, 98.336(3, γ, 90°, V, 7276.6(19) Å3, ρcalcd, 1.560 g cm-3, Z, 4, Rt (I > 2.0 σ (I, 0.0773, wR2 (all data, 0.2368, GOF, 1.079 (I > 2.0 σI
    • 2 (all data) = 0.2368, GOF = 1.079 (I > 2.0 σ(I)).
  • 30
    • 34250846159 scopus 로고    scopus 로고
    • 2 (all data) = 0.3204, GOF = 1.027 (I > 2.0 σ(I)).
    • 2 (all data) = 0.3204, GOF = 1.027 (I > 2.0 σ(I)).
  • 31
    • 34250903889 scopus 로고    scopus 로고
    • Crystallographic data for 3: C97H69Cl 3Cu3N6O16, Mw, 1871.55, triclinic, space group P1 (no. 2, a, 11.668(7, b, 19.070(12, c, 19.801(12) Å, α, 69.599(9, β, 87.517(10, γ, 84.319(10)°, V, 4109(4) Å3, ρcalcd, 1.513 g cm-3, Z, 2, R1, 0.0982 (I > 2.0 σ(I, wR2 (all data, 0.3117, GOF, 1.060 (I > 2.0 σ(I, CCDC-627140 (1, CCDC-627141 (2, and CCDC-627142 (3) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via
    • 2 (all data) = 0.3117, GOF = 1.060 (I > 2.0 σ(I)). CCDC-627140 (1), CCDC-627141 (2), and CCDC-627142 (3) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_ request/cif.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.