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Crystallographic data for 1: C81H58Cl 5N6Ni3O15, Mw, 1708.71, monoclinic, space group P21/c (no. 14, a, 11.4510(17, b, 20.120(3, c, 31.920(5) Å, α, 90, β, 98.336(3, γ, 90°, V, 7276.6(19) Å3, ρcalcd, 1.560 g cm-3, Z, 4, Rt (I > 2.0 σ (I, 0.0773, wR2 (all data, 0.2368, GOF, 1.079 (I > 2.0 σI
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2 (all data) = 0.2368, GOF = 1.079 (I > 2.0 σ(I)).
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30
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34250846159
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2 (all data) = 0.3204, GOF = 1.027 (I > 2.0 σ(I)).
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2 (all data) = 0.3204, GOF = 1.027 (I > 2.0 σ(I)).
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Crystallographic data for 3: C97H69Cl 3Cu3N6O16, Mw, 1871.55, triclinic, space group P1 (no. 2, a, 11.668(7, b, 19.070(12, c, 19.801(12) Å, α, 69.599(9, β, 87.517(10, γ, 84.319(10)°, V, 4109(4) Å3, ρcalcd, 1.513 g cm-3, Z, 2, R1, 0.0982 (I > 2.0 σ(I, wR2 (all data, 0.3117, GOF, 1.060 (I > 2.0 σ(I, CCDC-627140 (1, CCDC-627141 (2, and CCDC-627142 (3) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via
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2 (all data) = 0.3117, GOF = 1.060 (I > 2.0 σ(I)). CCDC-627140 (1), CCDC-627141 (2), and CCDC-627142 (3) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_ request/cif.
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33
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