SCOPUS 정보 검색 플랫폼

Chemistry - A European Journal

Volumn 13, Issue 17, 2007, Pages 4859-4872

Oligospiroketals as novel molecular rods

(3) Wessig, Pablo a Möllnitz, Kristian a Eiserbeck, Christiane a

a HUMBOLDT UNIVERSITY (Germany)

Author keywords

Cyclization; Ketalization; Molecular rods; Solubility; Spiro compounds

Indexed keywords

CARBOXYLIC ACIDS; CYCLIZATION; KETONES; SOLUBILITY; SYNTHESIS (CHEMICAL);

KETALIZATION; MOLECULAR RODS; OLIGOSPIROKETALS; SPIRO COMPOUNDS;

MOLECULAR DYNAMICS;

SPIRO COMPOUND;

ARTICLE; CHEMICAL STRUCTURE; CHEMISTRY; CONFORMATION; SYNTHESIS;

MOLECULAR CONFORMATION; MOLECULAR STRUCTURE; SPIRO COMPOUNDS;

EID: 34250312862 PISSN: 09476539 EISSN: 15213765 Source Type: Journal
DOI: 10.1002/chem.200700108 Document Type: Article

Times cited : (26)

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- Crystal data for 14a: C30H44O8, M, 532.65, monoclinic, Cc, a, 42.185(7, b, 5.9379(15, c, 11.2199(19) Å, α, 90.0, β, 89.71(2, γ, 90.0°, V, 2810.4(10) Å3, T, 180(2) K, graphite monochromatized MO Kα radiation, λ, 0.71073 Å, Z, 2, ρcalcd, 1.259 Mg m-3, crystal size 0.40 × 0.32 × 0.12 mm3. Data collected on a STOE Ipds diffractometer, 2472 unique reflections, Rint, 0.0750, Refinement on F2, final residuals R1, 0.0340 for 1870 reflections with I>2σI, wR2, 0.0668 for all data. CCDC-636085 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif
- 2, final residuals R1 = 0.0340 for 1870 reflections with I>2σI), wR2 = 0.0668 for all data. CCDC-636085 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.

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