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11
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34250161013
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Crystal data for 1. C31H29N 4O4Cl3Co, Mr, 686.86, monoclinic, space group I2/a, 15, a, 9.352(5, b, 15.145(5, c, 26.961(5) Å3, β, 54.240(5)°, V, 3099(2) Å3, Z, 4, Dcalcd, 1-47 g cm-1, μ(Mo Kα, 0.855 mm-1. 5348 unique reflections. Final residuals were R1, 0.055, wR2, 0.138 and GOF, 0.828 for 256 parameters and 2062 reflections (I net > 2σInet, CCDC-640931
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net)). CCDC-640931.
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12
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0000573906
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a) S. R. Batten, B. F. Hoskins, R. Robson, J. Am. Chem. Soc. 1995, 117, 5385.
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b) S. R. Batten, B. F. Hoskins, B. Moubaraki, K. S. Murray, R. Robson, Chem. Commun. 2000, 1095.
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d) K. Biradha, M. Fujita, Angew. Chem., Int. Ed. 2002, 41, 3392.
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0035820126
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Lin, C.2
Murillo, C.A.3
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20
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11344285784
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d) J. P. H. Charmant, A. H. M. Monowar Jahan, N. C. Norman, A. Guy Orpen, T. J. Podesta, CrystEngComm 2004, 6, 29.
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Charmant, J.P.H.1
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Norman, N.C.3
Guy Orpen, A.4
Podesta, T.J.5
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21
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34250162958
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Crystal data for 2. C80H86N 14O16Co3, Mr, 1676.4, monoclinic, space group P21/c, 14, a, 10.4230(3, b, 15.4308(5, c, 26.7556(9) Å, β, 77.2110(10)°, V, 4196.49(10) Å3, Z, 2, Dcalcd, 1.33 g cm-1, μ(Mo Kα, 0.658 mm-1. 14738 unique reflections. Final residuals were R 1, 0.056, wR2, 0.115 and GOF, 0.741 for 528 parameters and 3857 reflections (Inet > 2σInet, CCDC-640932
-
net)). CCDC-640932.
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23
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34250191917
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Supporting Information is available electronically on the CSJ-Journal Web site, http://www.csj.jp/journals/chem-lett/ index.html.
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Supporting Information is available electronically on the CSJ-Journal Web site, http://www.csj.jp/journals/chem-lett/ index.html.
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