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Volumn 36, Issue 5, 2007, Pages 634-635

Synthesis of highly functionalized alkenylphosphines by Lewis acid-mediated silylphosphination of substituted propiolates

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EID: 34250165383 PISSN: 03667022 EISSN: None Source Type: Journal
DOI: 10.1246/cl.2007.634 Document Type: Article

Times cited : (18)

References (16)

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- Dimethyl acetylenedicarboxylate was reported to react directly with silicon-phosphorus bond of a heterocyclic sillylphosphine: S. Haber, M. Schmitz, U. Bergsträßer, J. Hoffmann, M. Regitz, Chem. Eur. J. 1999, 5, 1581
- Dimethyl acetylenedicarboxylate was reported to react directly with silicon-phosphorus bond of a heterocyclic sillylphosphine: S. Haber, M. Schmitz, U. Bergsträßer, J. Hoffmann, M. Regitz, Chem. Eur. J. 1999, 5, 1581.

10
- 34250188181
- 13C NMR comparison with alkynylketone adducts reported in Ref. 4. The similarity of their magnitude of the coupling constants showed that 3a and 3b also have the same regio- and stereochemistry as the reported examples.
- 13C NMR comparison with alkynylketone adducts reported in Ref. 4. The similarity of their magnitude of the coupling constants showed that 3a and 3b also have the same regio- and stereochemistry as the reported examples.

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14
- 34250180655
- 3/n-hexane = 1/3 for 3c) to give the corresponding silylphosphine adduct.
- 3/n-hexane = 1/3 for 3c) to give the corresponding silylphosphine adduct.

15
- 34250163650
- The olefinic carbon signals with a relatively large coupling constant have been assigned as the carbon at 3-position (adjacent to the phosphorus) in the case of related silylphosphinated alkynyl ketones.4 However, our HMQC and HMBC analyses of 3a, 3d, and 3i revealed that these doublet signals with relatively large coupling constants are certainly assigned as the carbon adjacent to Si, whereas the signals with relatively small coupling constants are assigned as the carbon adjacent to P.7,12
- 7,12

16
- 34250220398
- Supporting Information is available electronically on the CSJ-Journal Web site, http://www.csj.jp/journals/chem-lett/ index.html.
- Supporting Information is available electronically on the CSJ-Journal Web site, http://www.csj.jp/journals/chem-lett/ index.html.

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.