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-1. The simulated and experimental XRPD patterns of 1 were in good agreement, which confirms the homogeneity of the compound products (see Fig. S3). Notes: Perchlorate salts of metal complexes are potentially explosive and should be handled with care.
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note
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int = 0.0243). Structure solution and refinement based on 6966 observed reflections with I > 2σ(I) and 625 parameters gave final R = 0.0430, wR = 0.1152 and S = 1.007. All of the calculations were performed by the SHELXTL™ 5 program. Crystallographic data in cif format have been deposited with the Cambridge Crystallographic Data Center, CCDC No. 632881 for 1.
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