Synthesis and characterization of vanadium(IV) complexes with cis-inositol in aqueous solution and in the solid-state

Inorganic Chemistry

Volumn 46, Issue 10, 2007, Pages 3903-3915

  Morgenstern, Bernd ^a   Kutzky, Barbara ^a   Neis, Christian ^a   Stucky, Stefan ^a   Hegetschweiler, Kaspar ^a   Garribba, Eugenio ^b   Micera, Giovanni ^b  

^a SAARLAND UNIVERSITY   (Germany)

^b UNIVERSITY OF SASSARI   (Italy)

Author keywords

[No Author keywords available]

Indexed keywords

INOSITOL; LIGAND; OXYGEN; VANADIUM DERIVATIVE; WATER;

ARTICLE; CHEMICAL STRUCTURE; CHEMISTRY; ELECTROCHEMISTRY; ELECTRON SPIN RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PHYSICAL CHEMISTRY; POTENTIOMETRY; SOLUTION AND SOLUBILITY; SYNTHESIS; X RAY DIFFRACTION;

CHEMISTRY, PHYSICAL; ELECTROCHEMISTRY; ELECTRON SPIN RESONANCE SPECTROSCOPY; INOSITOL; LIGANDS; MAGNETIC RESONANCE SPECTROSCOPY; MODELS, MOLECULAR; OXYGEN; POTENTIOMETRY; SOLUTIONS; VANADIUM COMPOUNDS; WATER; X-RAY DIFFRACTION;

EID: 34249707729     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic0618504     Document Type: Article

References (66)

1. Rehder, D. In Metal Ions in Biological Systems; Sigel, A.; Sigel, H., Eds.; Marcel Dekker: New York, 1995; Vol. 31, pp 1-43.
2. Crans, D. C.; Smee, J. J.; Gaidamauskas, E.; Yang, L. Chem. Rev. 2004, 104, 849-902 and references therein.
3. Pecoraro, V. L.; Slebodnick, C. A.; Hamstra, B. J. In Vanadium Compounds: Chemistry, Biochemistry, and Therapeutic Applications; Tracey, A. S.; Crans, D. C. Eds.; ACS Symposium Series 711, Washington, DC, 1998; pp 157-167.
4. Robson, R. L.; Eady, R. R.; Richardson, T. H.; Miller, R. W.; Hawkins, M.; Postgate, J. R. Nature 1986, 322, 388-390.
5. Eady, R. R. In Metal Ions in Biological Systems; Sigel, A.; Sigel, H., Eds.; Marcel Dekker: New York, 1995; Vol. 31, pp 363-405 and references therein.
6. Smith, M. J.; Ryan, D. E.; Nakanishi, K.; Frank, P.; Hodgson, K. O. In Metal Ions in Biological Systems; Sigel, A.; Sigel, H., Eds.; Marcel Dekker: New York, 1995; Vol. 31, pp 423-490.
7. Shechter, Y.; Karlish, S. J. D. Nature 1980, 284, 556-558.
8. Thompson, K. H.; McNeill, J. H.; Orvig, C. Chem. Rev. 1999, 99, 2561-2571 and references therein.
9. Shechter, Y.; Goldwaser, I.; Mironchik, M.; Fridkin, M.; Gefel, D. Coord. Chem. Rev. 2003, 237, 3-11.
10. (a) Bayer, E.; Kneifel, H. Z. Naturforsch. B 1972, 27, 207-207.
11. (b) Kneifel, H.; Bayer, E. Angew. Chem. Int. Ed. Engl. 1973, 12, 508-509.
12. (a) Carrondo, M. A. A. F. de C. T.; Duarte, M. T. L. S.; Costa Pessoa, J.; Silva, J. A. L.; Fraústo da Silva, J. J. R.; Vaz, M. C. T. A.; Vilas-Boas, L. F. J. Chem. Soc. Chem. Commun. 1988, 1158-1159.
13. (b) Carrondo, M. A. A. F. de C. T.; Duarte, M. T. L. S.; Fraústo da Silva, J. J. R.; da Silva, J. A. L. Struct. Chem. 1992, 3, 113-119.
14. (a) Smith, P. D.; Berry, R. E.; Harben, S. M.; Beddoes, R. L.; Helliwell, M.; Collison, D.; Garner, C. D. J. Chem. Soc. Dalton Trans. 1997, 4509-4516.
15. (b) Berry, R. E.; Armstrong, E. M.; Beddoes, R. L.; Collison, D.; Ertok, S. N.; Helliwell, M.; Garner, C. D. Angew. Chem. Int. Ed. 1999, 38, 795-797.
16. (a) Vergopoulos, V.; Jantzen, S.; Rodewald, D.; Rehder D. J. Chem. Soc. Chem. Commun. 1995, 377-378.
17. (b) Ludwig, E.; Hefele, H.; Uhlemann, E.; Weller, F.; Kläui, W. Z. Anorg. Allg. Chem. 1995, 621, 23-28.
18. (c) Hefele, H.; Ludwig, E.; Uhlemann, E.; Weller, F. Z. Anorg. Allg. Chem. 1995, 621, 1973-1976.
19. (d) Klich, P. R.; Daniher, A. T.; Challen, P. R.; McConville, D. B.; Youngs, W. J. Inorg. Chem. 1996, 35, 347-356.
20. (e) Kondo, M.; Minakoshi, S.; Iwata, K.; Shimizu, T.; Matsuzaka, H.; Kamigata, N.; Kitagawa, S. Chem. Lett. 1996, 489-490.
21. (f) Kang, B. S.; Wang, X. J.; Su, C. Y.; Liu, H. Q.; Wen, T. B.; Liu, Q. T. Transition Met. Chem. 1999, 24, 712-717.
22. (g) Paine, T. K.; Weyhermüller, T.; Bill, E.; Bothe, E.; Chaudhuri, P. Eur. J. Inorg. Chem. 2003, 4299-4307.
23. (h) Paine, T. K.; Weyhermüller, T.; Slep, L. D.; Neese, F. Bill, E.; Bothe, E.; Wieghardt, K.; Chaudhuri, P. Inorg. Chem. 2004, 43, 7324-7338.
24. Allen, F. H.; Kennard, O. Chem. Des. Autom. News 1993, 8, 31-37.
25. Morgenstern, B.; Steinhauser, S.; Hegetschweiler, K.; Garribba, E.; Micera, G.; Sanna, D.; Nagy, L. Inorg. Chem. 2004, 43, 3116-3126.
26. Hegetschweiler, K. Chem. Soc. Rev. 1999, 28, 239-249.
27. Hegetschweiler, K.; Gramlich, V.; Ghisletta, M.; Samaras, H. Inorg. Chem. 1992, 31, 2341-2346.
28. Ghisletta, M.; Hausherr-Primo, L.; Gajda-Schrantz, K.; Machula, G.; Nagy, L.; Schmalle, H. W.; Rihs, G.; Endres, F.; Hegetschweiler, K. Inorg. Chem. 1998, 37, 997-1008.
29. Hegetschweiler, K.; Ghisletta, M.; Fässler, T. F.; Nesper, R.; Schmalle, H. W.; Rihs, G. Inorg. Chem. 1993, 32, 2032-2041.
30. (a) Hegetschweiler, K.; Kradolfer, T.; Gramlich, V.; Hancock, R. D. Chem. - Eur. J. 1995, 1, 74-88.
31. (b) Hegetschweiler, K.; Raber, T.; Reiss, G. J.; Frank, W.; Wörle, M.; Currao, A.; Nesper, R.; Kradolfer, T. Angew. Chem., Int. Ed. Engl. 1997, 36, 1964-1966.
32. Branca, M.; Micera, G.; Dessí, A.; Sanna, D.; Raymond, K. N. Inorg. Chem. 1990, 29, 1586-1589.
33. Hancock, R. D.; Hegetschweiler, K. J. Chem. Soc. Dalton Trans. 1993, 2137-2140.
34. Shannon, R. D. Acta. Crystallogr. 1976, A32, 751-767.
35. Hegetschweiler, K.; Hausherr-Primo, L.; Koppenol, W. H.; Gramlich, V.; Odier, L.; Meyer, W.; Winkler, H.; Trautwein, A. X. Angew. Chem., Int. Ed. Engl. 1995, 34, 2242-2243.
36. Morgenstern, B.; Sander, J.; Huch, V.; Hegetschweiler, K. Inorg. Chem. 2001, 40, 5307-5310.
37. Steinhauser, S.; Heinz, U.; Bartholomä, M.; Weyhermüller, T.; Nick, H.; Hegetschweiler, K. Eur. J. Inorg. Chem. 2004, 4177-4192.
38. Gans, P.; Sabatini, A.; Vacca, A. Talanta 1996, 43, 1739-1753.
39. Smith, R. M.; Martell, A. E.; Motekaitis, R. J. Critically Selected Stability Constants of Metal Complexes; NIST Standard Reference Database 46, version 8.0; NIST: Gaithersburg, MD, 2004.
40. Henry, R. P.; Mitchell, P. C. H.; Prue, J. E. J. Chem. Soc. Dalton Trans. 1973, 1156-1159.
41. (a) Komura, A.; Hayashi, M.; Imanaga, H. Bull. Chem. Soc. Jpn. 1977, 50, 2927-2931.
42. (b) Vilas Boas, L. F.; Costa Pessoa J. In Comprehensive Coordination Chemistry; Wilkinson, G.; Gillard, R. D.; McCleverty J. A., Eds.; Pergamon Press: Oxford, 1987; Vol. 3, pp 453-583.
43. Davies, C. W. J. Chem. Soc. 1938, 2093-2098.
44. (a) Binstead, R. A.; Jung, B.; Zuberbühler, A. D. SPECFIT/32, Version 3.0, Spectrum Software Associates: Marlborough, MA 01752, 2000.
45. (b) Gampp, H.; Maeder, M.; Meyer, C. J.; Zuberbühler, A. D. Talanta 1985, 32, 95-101.
46. WINEPR SimFonia, version 1.25, Bruker Analytische Messtechnik GmbH, Karlsruhe, Germany, 1996.
47. A corresponding ortho-pentanoate has been described. See Biamonte, M. A.; Vasella, A. Helv. Chim. Acta. 1998, 81, 695-717.
48. (a) Sheldrick, G. M. SHELXS-97, Program for Crystal Structure Solution, Göttingen, Germany, 1997.
49. (b) Sheldrick, G. M. SHELXL-97, Program for Crystal Structure Refinement, Göttingen, Germany, 1997.
50. 2O with L = ino, tmci.
51. Smith, T. D.; Pilbrow, J. R. Coord. Chem. Rev. 1974, 13, 173-278.
52. Hegetschweiler, K.; Ghisletta, M.; Gramlich, V. Inorg. Chem. 1993, 32, 2699-2704.
53. Hedinger, R.; Ghisletta, M.; Hegetschweiler, K.; Tóth, E.; Merbach, A. E.; Sessoli, R.; Gatteschi, D.; Gramlich, V. Inorg. Chem. 1998, 37, 6698-6705.
54. Chasteen, N. D. In Biological Magnetic Resonance; Berliner, L. J.; Reuben, J., Eds.; Plenum Press: New York, 1981; Vol. 3, pp 53-119.
55. Hausherr-Primo, L.; Hegetschweiler, K.; Rüegger, H.; Odier, L.; Hancock, R. D.; Schmalle, H. W.; Gramlich, V. J. Chem. Soc. Dalton Trans. 1994, 1689-1701.
56. 2O revealed a value of 59.5° for the taci complex and a value of exactly 60.0° for the two centrosymmetric tdci complexes, provided that the two triangles oriented perpendicular to the (pseudo) threefold rotational axis are considered.
57. Petrella, A. J.; Craig, D. C.; Lamb, R. N.; Raston, C. L.; Roberts, N. K. Dalton Trans. 2003, 4590-4597.
58. Bode, H.; Teufer, G. Acta. Crystallogr. 1956, 9, 929-933.
59. (a) Armstrong, D. R.; Clegg, W.; Drummond, A. M.; Liddle, S. T.; Mulvey, R. E. J. Am. Chem. Soc. 2000, 122, 11117-11124.
60. (b) Geier, J.; Grützmacher, H. Chem. Commun. 2003, 2942-2943.
61. (c) Geier, J.; Rüegger, H.; Grützmacher, H. Dalton Trans. 2006, 129-136.
62. (d) Fischer, R.; Görls, H.; Walther, D. Eur. J. Inorg. Chem. 2004, 1243-1252.
63. (e) MacDougall, D. J.; Noll, B. C.; Henderson, K. W. Inorg. Chem. 2005, 44, 1181-1183.
64. Jezierski, A.; Raynor, J. B. J. Chem. Soc. Dalton Trans. 1981, 1-7.
65. Desideri, A.; Raynor, J. B.; Diamantis, A. A. J. Chem. Soc. Dalton Trans. 1978, 423-426.
66. Olk, R. M.; Dietzsch, W.; Kirmse, R.; Stach, J.; Hoyer, E.; Golic, L. Inorg. Chim. Acta. 1987, 128, 251-259.