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85088079362
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note
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N) were found. A pulse delay of 10 s thus ensured complete relaxation and allowed a quantitative evaluation of the integrated spectrum.
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53
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85088078252
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note
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2O. Using the pD dependence of the chemical shifts of taci, corresponding values of 6.07, 7.32, and 8.84 were calculated by a least-squares refinement (32 data points) as described in ref 7.
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1842811639
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note
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3+ within the experimental error.
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