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Crystal data for (HgBr2)3(As4S 4)2: M, 1937.1 g/mol, monoclinic, space group P2 1/c, lattice constants (refined from X-ray powder diffraction data, a, 9.593(5) Å, b, 11.395(5) Å, c, 13.402(5) Å, β= 107.27(3)°, V, 1399(1) Å3, Z, 2, μ, 35.0 cm -1, θ-range, 2.22-25.03°; reflections collected: 14504, reflections independent: 2470, Rint: 0.0632, Rσ: 0.0423, parameters: 115, Goof: 0.949, R1,(all data, 0.0525, wR 2(all data, 0.0863, largest residual peaks: 1.358 and, 1.070 eÅ-3. Refinement on F2 with SHELX97 [16, Further details on the crystal structure investigations may be obtained from the Fachinformationszentrum Karlsruhe, 76344 Eggenstein-Leopoldshafen, Germany (fax:, 49) 7247-808-666; E-mail: crysdata@fiz-karlsruhe.de, on quoting the depository number CSD-41762
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