-
1
-
-
0038681019
-
-
Schultz, M.; Boncella, J. M.; Berg, D. J.; Tilley, T. D.; Andersen, R. A. Organometallics 2002, 21, 460-472.
-
(2002)
Organometallics
, vol.21
, pp. 460-472
-
-
Schultz, M.1
Boncella, J.M.2
Berg, D.J.3
Tilley, T.D.4
Andersen, R.A.5
-
2
-
-
32544443625
-
-
Walter, M. D.; Schultz, M.; Andersen, R. A. New J. Chem. 2006, 30, 238-246.
-
(2006)
New J. Chem
, vol.30
, pp. 238-246
-
-
Walter, M.D.1
Schultz, M.2
Andersen, R.A.3
-
3
-
-
33745745448
-
-
Walter, M. D.; Berg, D. J.; Andersen, R. A. Organometallics 2006, 25, 3228-3237.
-
(2006)
Organometallics
, vol.25
, pp. 3228-3237
-
-
Walter, M.D.1
Berg, D.J.2
Andersen, R.A.3
-
4
-
-
0038337812
-
-
Berg, D. J.; Boncella, J. M.; Andersen, R. A. Organometallics 2002, 27, 4622-4631.
-
(2002)
Organometallics
, vol.27
, pp. 4622-4631
-
-
Berg, D.J.1
Boncella, J.M.2
Andersen, R.A.3
-
5
-
-
0038401487
-
-
Rosen, R. K.; Andersen, R. A.; Edelstein, N. M. J. Am. Chem. Soc. 1990, 112, 4588-4590.
-
(1990)
Am. Chem. Soc
, vol.112
, pp. 4588-4590
-
-
Rosen, R.K.1
Andersen, R.A.2
Edelstein, N.M.J.3
-
6
-
-
23844484576
-
-
Veauthier, J. M.; Schelter, E. J.; Kuehl, C. J.; Clark, A. E.; Scott, B. L.; Morris, D. E.; Martin, R. L.; Thompson, J. D.; Kiplinger, J. L.; John, K. D. Inorg. Chem. 2005, 44, 5911-5920.
-
(2005)
Inorg. Chem
, vol.44
, pp. 5911-5920
-
-
Veauthier, J.M.1
Schelter, E.J.2
Kuehl, C.J.3
Clark, A.E.4
Scott, B.L.5
Morris, D.E.6
Martin, R.L.7
Thompson, J.D.8
Kiplinger, J.L.9
John, K.D.10
-
7
-
-
0141790827
-
-
Kuehl, C. J.; Da Re, R. E.; Scott, B. L.; Morris, D. E.; John, K. D. Chem. Commun. 2003, 2336-2337.
-
(2003)
Chem. Commun
, pp. 2336-2337
-
-
Kuehl, C.J.1
Da Re, R.E.2
Scott, B.L.3
Morris, D.E.4
John, K.D.5
-
8
-
-
30344474022
-
-
Booth, C. H.; Walter, M. D.; Daniel, M.; Lukens, W. W.; Andersen, R. A. Phys. Rev. Lett. 2005, 95, 267202.
-
(2005)
Phys. Rev. Lett
, vol.95
, pp. 267202
-
-
Booth, C.H.1
Walter, M.D.2
Daniel, M.3
Lukens, W.W.4
Andersen, R.A.5
-
9
-
-
0002627202
-
-
Recknagel, A.; Noltemeyer, M.; Edelmann, F. T. J. Organomet. Chem. 1991, 410, 53-61.
-
(1991)
J. Organomet. Chem
, vol.410
, pp. 53-61
-
-
Recknagel, A.1
Noltemeyer, M.2
Edelmann, F.T.3
-
10
-
-
33751393344
-
-
Moore, J. A.; Cowley, A. H.; Gordon, M. C. Organometallics 2006, 25, 5207-5209.
-
(2006)
Organometallics
, vol.25
, pp. 5207-5209
-
-
Moore, J.A.1
Cowley, A.H.2
Gordon, M.C.3
-
11
-
-
34248381942
-
-
Trifonov, A. A.; Kirillov, E. N.; Bochkarev, M. N.; Schumann, H.; Muehle, S. Russ. Chem. Bull. 1999, 48, 381-384.
-
(1999)
Russ. Chem. Bull
, vol.48
, pp. 381-384
-
-
Trifonov, A.A.1
Kirillov, E.N.2
Bochkarev, M.N.3
Schumann, H.4
Muehle, S.5
-
12
-
-
0038661937
-
-
Trifonov, A. A.; Kurskii, Y. A.; Bochkarev, M. N.; Muehle, S.; Dechert, S.; Schumann, H. Russ. Chem. Bull. 2003, 52, 601-606.
-
(2003)
Russ. Chem. Bull
, vol.52
, pp. 601-606
-
-
Trifonov, A.A.1
Kurskii, Y.A.2
Bochkarev, M.N.3
Muehle, S.4
Dechert, S.5
Schumann, H.6
-
13
-
-
22544435523
-
-
Trifonov, A. A.; Fedorova, E. A.; Ikorskii, V. N.; Kurskii, Y. A.; Dechert, S.; Schumann, H.; Bochkarev, M. N. Eur. J. Inorg. Chem. 2005, 2812-2818.
-
(2005)
Eur. J. Inorg. Chem
, pp. 2812-2818
-
-
Trifonov, A.A.1
Fedorova, E.A.2
Ikorskii, V.N.3
Kurskii, Y.A.4
Dechert, S.5
Schumann, H.6
Bochkarev, M.N.7
-
14
-
-
0034795990
-
-
Trifonov, A. A.; Kirillov, E. N.; Dechert, S.; Schumann, H.; Bochkarev, M. N. Eur. J. Inorg. Chem. 2001, 2509-2514.
-
(2001)
Eur. J. Inorg. Chem
, pp. 2509-2514
-
-
Trifonov, A.A.1
Kirillov, E.N.2
Dechert, S.3
Schumann, H.4
Bochkarev, M.N.5
-
15
-
-
33645304676
-
-
Trifonov, A. A.; Fedorova, E. A.; Fukin, G. K.; Druzhkov, N. O.; Bochkarev, M. N. Angew. Chem. 2004, 116, 5155-5158.
-
(2004)
Angew. Chem
, vol.116
, pp. 5155-5158
-
-
Trifonov, A.A.1
Fedorova, E.A.2
Fukin, G.K.3
Druzhkov, N.O.4
Bochkarev, M.N.5
-
16
-
-
33645278647
-
-
Trifonov, A. A.; Fedorova, E. A.; Fukin, G. K.; Baranov, E. V.; Druzhkov, N. O.; Bochkarev, M. N. Chem. Eur. J. 2006, 12, 2752-2757.
-
(2006)
Chem. Eur. J
, vol.12
, pp. 2752-2757
-
-
Trifonov, A.A.1
Fedorova, E.A.2
Fukin, G.K.3
Baranov, E.V.4
Druzhkov, N.O.5
Bochkarev, M.N.6
-
17
-
-
0001021241
-
-
McPherson, A. M.; Fieselmann, B. F.; Lichtenberger, D. L.; McPherson, G. L.; Stucky, G. D. J. Am. Chem. Soc. 1979, 101, 3425-3430.
-
(1979)
J. Am. Chem. Soc
, vol.101
, pp. 3425-3430
-
-
McPherson, A.M.1
Fieselmann, B.F.2
Lichtenberger, D.L.3
McPherson, G.L.4
Stucky, G.D.5
-
19
-
-
0000981079
-
-
Kaupp, M.; Stall, H.; Preuss, H.; Kaim, W.; Stahl, T.; van Koten, G.; Wissing, E.; Smeets, W. J. J.; Spek, A. L. J. Am. Chem. Soc. 1991, 113, 5606-5618.
-
(1991)
J. Am. Chem. Soc
, vol.113
, pp. 5606-5618
-
-
Kaupp, M.1
Stall, H.2
Preuss, H.3
Kaim, W.4
Stahl, T.5
van Koten, G.6
Wissing, E.7
Smeets, W.J.J.8
Spek, A.L.9
-
23
-
-
34248337712
-
-
1
-
1
-
-
-
-
24
-
-
0001609866
-
-
Tilley, T. D.; Andersen, R. A.; Spencer, B.; Zalkin, A. Inorg. Chem. 1982, 21, 2647-2649.
-
(1982)
Inorg. Chem
, vol.21
, pp. 2647-2649
-
-
Tilley, T.D.1
Andersen, R.A.2
Spencer, B.3
Zalkin, A.4
-
25
-
-
0000771830
-
-
Huige, C. J. M.; Spek, A. L.; de Boer, J. L. Acta Crystallogr. 1983, C41, 113-116.
-
(1983)
Acta Crystallogr
, vol.C41
, pp. 113-116
-
-
Huige, C.J.M.1
Spek, A.L.2
de Boer, J.L.3
-
26
-
-
33744959375
-
-
Carlson, C. N.; Kuehl, C. J.; Da Re, R. E.; Veauthier, J. M.; Schelter, E. J.; Milligan, A. E.; Scott, B. L.; Bauer, E. D.; Thompson, J. D.; Morris, D. E.; John, K. D. J. Am. Chem. Soc. 2006, 128, 7230-7241.
-
(2006)
J. Am. Chem. Soc
, vol.128
, pp. 7230-7241
-
-
Carlson, C.N.1
Kuehl, C.J.2
Da Re, R.E.3
Veauthier, J.M.4
Schelter, E.J.5
Milligan, A.E.6
Scott, B.L.7
Bauer, E.D.8
Thompson, J.D.9
Morris, D.E.10
John, K.D.11
-
27
-
-
34248396198
-
-
Variable-temperature Yb Lm-edge XANES studies on the compounds reported here and on other bipy-X compounds will be published in due course (Booth, C. H. Personal communication).
-
Variable-temperature Yb Lm-edge XANES studies on the compounds reported here and on other bipy-X compounds will be published in due course (Booth, C. H. Personal communication).
-
-
-
-
28
-
-
34248340270
-
-
The isotropic chemical shifts (δiso, δobs, δdia) have not been determined, since the diamagnetic analogues to the molecules presented in this paper, e.g, C 5Me5)2Ca(dad(R′)-R, have not been prepared. However, approximate isotropic shifts (δiso) using the chemical shifts of (C5Me5)2-Yb(py) 2 and the free dad(R′)-R ligands have been calculated see the Supporting Information, Errors introduced by nonideal reference compounds are expected to be small for ′H NMR data
-
2 and the free dad(R′)-R ligands have been calculated (see the Supporting Information). Errors introduced by nonideal reference compounds are expected to be small for ′H NMR data.
-
-
-
-
29
-
-
11844273890
-
-
Maron, L.; Werkema, E. L.; Perrin, L.: Eisenstein, O.; Andersen, R. A. J. Am. Chem. Soc. 2005, 127, 279-292.
-
(2005)
J. Am. Chem. Soc
, vol.127
, pp. 279-292
-
-
Maron, L.1
Werkema, E.L.2
Perrin, L.3
Eisenstein, O.4
Andersen, R.A.5
-
30
-
-
25444458609
-
-
Zi, G.; Blosch, L. L.; Jia, L.; Andersen, R. A. Organometallics 2005, 24, 4602-4612.
-
(2005)
Organometallics
, vol.24
, pp. 4602-4612
-
-
Zi, G.1
Blosch, L.L.2
Jia, L.3
Andersen, R.A.4
-
33
-
-
0342311319
-
-
(c) Horrocks, W. D.; Taylor, R. C.; LaMar, G. N. J. Am. Chem. Soc. 1964, 86, 3031-3038.
-
(1964)
Am. Chem. Soc
, vol.86
, pp. 3031-3038
-
-
Horrocks, W.D.1
Taylor, R.C.2
LaMar, G.N.J.3
-
34
-
-
2942755178
-
-
(d) LaLancette, E. A.; Eaton, D. R.; Benson, R. E.; Phillips, W. D. J. Am. Chem. Soc. 1962, 84, 3968-3970.
-
(1962)
J. Am. Chem. Soc
, vol.84
, pp. 3968-3970
-
-
LaLancette, E.A.1
Eaton, D.R.2
Benson, R.E.3
Phillips, W.D.4
-
35
-
-
84967110193
-
Probing Spin Densities by Use of NMR Spectroscopy
-
Miller, J. S, Drillon, M, Eds, Wiley-VCH: Weinheim, Germany, and references cited therein
-
Köhler, F. H. Probing Spin Densities by Use of NMR Spectroscopy. In Magnetism: Molecules to Materials. Models and Experiments; Miller, J. S., Drillon, M., Eds.; Wiley-VCH: Weinheim, Germany, 2001; pp 379-430, and references cited therein.
-
(2001)
Magnetism: Molecules to Materials. Models and Experiments
, pp. 379-430
-
-
Köhler, F.H.1
-
36
-
-
0002069684
-
NMR-spectroscopy of organo-f-element and prelanthanoid complexes: Some current trends
-
Marks, T. J, Fragalà, I. L, Eds, D. Reidel: Dordrecht, The Netherlands
-
Fischer, R. D. NMR-spectroscopy of organo-f-element and prelanthanoid complexes: some current trends. In Fundamental and Technological Aspects of Organo-f-Element Chemistry; Marks, T. J., Fragalà, I. L., Eds.; D. Reidel: Dordrecht, The Netherlands, 1985; pp 277-326.
-
(1985)
Fundamental and Technological Aspects of Organo-f-Element Chemistry
, pp. 277-326
-
-
Fischer, R.D.1
-
37
-
-
0011674128
-
Lanthanide and Actinide Complexes
-
La Mar, G. N, Horrocks, W. D, Holm, R. H, Eds, Academic Press: New York
-
Fischer, R. D. Lanthanide and Actinide Complexes. In NMR of Paramagnetic Molecules; La Mar, G. N., Horrocks, W. D., Holm, R. H., Eds.; Academic Press: New York, 1973; pp 521-553.
-
(1973)
NMR of Paramagnetic Molecules
, pp. 521-553
-
-
Fischer, R.D.1
-
39
-
-
0001668776
-
-
Knorr, R.; Polzer, H.; Bischler, E. J. Am. Chem. Soc. 1975, 97, 643-644.
-
(1975)
J. Am. Chem. Soc
, vol.97
, pp. 643-644
-
-
Knorr, R.1
Polzer, H.2
Bischler, E.3
-
40
-
-
0011583998
-
-
Knorr, R.; Weiss, A.; Polzer, H.; Bischler, E. J. Am. Chem. Soc. 1975, 97, 644-646.
-
(1975)
J. Am. Chem. Soc
, vol.97
, pp. 644-646
-
-
Knorr, R.1
Weiss, A.2
Polzer, H.3
Bischler, E.4
-
42
-
-
0035743042
-
-
Heise, H.; Köhler, F. H.; Xie, X. J. Magn. Reson. 2001, 150, 198-206.
-
(2001)
J. Magn. Reson
, vol.150
, pp. 198-206
-
-
Heise, H.1
Köhler, F.H.2
Xie, X.3
-
43
-
-
0000797230
-
-
Lukens, W. W.; Beshouri, S. M.; Stuart, A. L.; Andersen, R. A. Organometallics 1999, 18, 1247-1252.
-
(1999)
Organometallics
, vol.18
, pp. 1247-1252
-
-
Lukens, W.W.1
Beshouri, S.M.2
Stuart, A.L.3
Andersen, R.A.4
-
46
-
-
34248362192
-
-
In all of the diazabutadiene complexes with (C5Me 5)2Yb, except the mesityl derivative just discussed, the chemical shift of the C5Me5 resonances moves downfield, passes through a minimum value at about -50 to -60°C, and then moves upfield as the temperature is decreased to -80°C. This nonlinear behavior is due to temperature-dependent processes whose populations and chemical shifts depend on temperature.32 The averaged chemical shift, δaV, is the weighted chemical shift of two nuclei, δav, aδA, bδB- If the populations are unequal, a ≠ b, then δav vs T-1 will be the sum of the individual δA vs T-1 and δB vs T-1 plots, which will be nonlinear if the populations change with temperature. Conversely, if a, b but δA
-
5 might be correlated to the motion of the N-heterocyclic base about the horizontal mirror plane; however, there is insufficient information in the line shape to delineate the physical process responsible.
-
-
-
-
47
-
-
0346004891
-
-
Clopath, P.; v. Zelewsky, A. Helv. Chim. Acta 1972, 55, 52-66.
-
Clopath, P.; v. Zelewsky, A. Helv. Chim. Acta 1972, 55, 52-66.
-
-
-
-
48
-
-
34248381941
-
-
2 Yb(dad-(H)-adamantyl) could not be reached, and the rotation barriers cannot be determined.
-
2 Yb(dad-(H)-adamantyl) could not be reached, and the rotation barriers cannot be determined.
-
-
-
-
50
-
-
18844384949
-
-
Wang, J.; Amos, R. I. J.; Frey, A. S. P.; Gardiner, M. G.; Cole, M. L.; Junk, P. C. Organometallics 2005, 24, 2259-2261.
-
(2005)
Organometallics
, vol.24
, pp. 2259-2261
-
-
Wang, J.1
Amos, R.I.J.2
Frey, A.S.P.3
Gardiner, M.G.4
Cole, M.L.5
Junk, P.C.6
-
53
-
-
0001388609
-
-
Tilley, T. D.; Boncella, J. M.; Berg, D. J.; Burns, C. J.; Andersen, R. A. Inorg. Synth. 1990, 27, 146-149.
-
(1990)
Inorg. Synth
, vol.27
, pp. 146-149
-
-
Tilley, T.D.1
Boncella, J.M.2
Berg, D.J.3
Burns, C.J.4
Andersen, R.A.5
-
54
-
-
84932888215
-
-
tom Dieck, H.; Franz, K.-D.; Majunke, W. Z. Naturforsch. 1975, 30b, 922-925.
-
(1975)
Z. Naturforsch
, vol.30 b
, pp. 922-925
-
-
tom Dieck, H.1
Franz, K.-D.2
Majunke, W.3
-
56
-
-
0000631570
-
-
tom Dieck, H.; Svoboda, M.; Greiser, T. Z. Naturforsch. 1981, 36b, 823-832.
-
(1981)
Naturforsch
, vol.36 b
, pp. 823-832
-
-
tom Dieck, H.1
Svoboda, M.2
Greiser, T.Z.3
-
57
-
-
34248341605
-
-
Ph.D. Thesis, Eberhard-Karls-Universität, Tübingen, Germany
-
Walker, I. Ph.D. Thesis, Eberhard-Karls-Universität, Tübingen, Germany, 2002.
-
(2002)
-
-
Walker, I.1
-
58
-
-
0033579627
-
-
Arduengo, A. J.; Krafczyk, R.; Schmutzler, R.; Craig, H. A.; Goerlich, J. R.; Marshall, W. J.; Unverzagt, M. Tetrahedron 1999, 55, 14523-14534.
-
(1999)
Tetrahedron
, vol.55
, pp. 14523-14534
-
-
Arduengo, A.J.1
Krafczyk, R.2
Schmutzler, R.3
Craig, H.A.4
Goerlich, J.R.5
Marshall, W.J.6
Unverzagt, M.7
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