Dimeric phosphinoboranes R′(Hal)B-PHR2 and some of their Reactions [1]

Zeitschrift fur Anorganische und Allgemeine Chemie

Volumn 633, Issue 5-6, 2007, Pages 917-926

  Jetzfellner, Ralf ^a   Nöth, Heinrich ^a   Paine, Robert T ^b  

^a UNIVERSITY OF MUNICH   (Germany)

^b UNIVERSITY OF NEW MEXICO   (United States)

Author keywords

1,3,2,4 Diphosphadiboracyclobutanes; Bicyclo 1.1.0 triphosphadibora pentane; Mass spectra; NMR; P lithiation; X ray crystallography

Indexed keywords

EID: 34248138980     PISSN: 00442313     EISSN: 15213749     Source Type: Journal    
DOI: 10.1002/zaac.200700070     Document Type: Article

References (39)

1. Contribution to the Chemistry of Boron, 266; for contribution 265 see U. Braun, H. Nöth, Eur. J. Inorg. Chem. 2007, submit-ted.
2. H. Nöth, R. T. Paine, Chem. Rev. 1995, 95, 343.
3. I. Haiduc, The Chemistry of Inorganic Ring Systems. Vol.1, Wiley Interscience, London, NewYork, Sydney, Toronto, 1970.
4. G. W. Parshall, The Chemistry of Boron and its Compounds, Editor: E. L. Muetterties, J. Wiley and Sons, New York, 1973, 617.
5. D. A. Armitage, Inorganic Rings and Cages, E. Arnold Publ. 1972, 109.
6. R. Jetzfellner, H. Nöth, R. T. Paine, Z. Anorg. Allg. Chem. 2007, 633, 548.
7. P. P. Power, Angew. Chem. 1990, 102, 527;
8. Angew. Chem. Int. Ed. Engl. 1990, 29, 481.
9. Detailed simulations have not been attempted since they would require a computer programme capable of handling a 22 spin system (Dr. K. Karaghiosoff, Dr. D. Stevenson).
10. 13C NMR spectrum was not be recorded.
11. D. Scheschkewitz, H. Amil, H. Gornitza, W. W. Schoeller, D. Bourissou, G. Bertrand, Angew. Chem. 2004, 116, 595;
12. Angew. Chem. Int. Ed. 2004, 43, 585.
13. H. Amil, L. Kranicar, H. Gornitzki, D. Bourissou, G. Bertrand, J. Am. Chem. Soc. 2004, 126, 1344.
14. R. A. Bartlett, H. V. R. Dias, X. Feng, P. P. Power, J. Am. Chem. Soc. 1989, 111, 1306.
15. S. J. Lancaster, A. J. Mountford, D. L. Hughes, M. Schormann, M. Bochmann, J. Organomet. Chem. 2003, 680, 193.
16. F. C. Alyea, A. Costin, G. Ferguson, G. T. Frey, R. G Goel, R. J. Restivo, J. Chem. Soc. Dalton Trans. 1975, 1294.
17. D. L. Thorn, J. C. Calabrese, J. Organomet. Chem. 1984, 272, 283.
18. P. Mura, J. Coord. Chem. 1999, 48, 503.
19. F. J. Hual, J. L. Atwood, J. Coord. Chem. 1999, 46, 505.
20. K. A. O. Starzewski, W. M. Kelly, A. Stumpf, D. Freitag, Angew. Chem. 1999, 111, 2588;
21. Angew. Chem. Int. Ed. 1999, 38, 2439.
22. W. P. Hul, H. Britzwanger, A. A. Broehus, H. J. Heres, A. J. von Linden, A. G. Orpen, Inorg. Chim. Acta 2002, 327, 147.
23. H. H. Karsch, G. Hanika, B. Huber, J. Riede, G. Müller, J. Organomet. Chem. 1989, 361, C25.
24. H. Nöth, W. Schrägle, Chem. Ber. 1965, 98, 352.
25. X. Feng, M. M. Olmstead, P. P. Power, Inorg. Chem. 1986, 25, 4615.
26. D. C. Pestana, P. P. Power, J. Am. Chem. Soc. 1991, 113, 8426.
27. W. Gee, R. A. Shaw, B. C. Smith, G. J. Bullen, Proc. Chem. Soc. 1961, 432.
28. W. C. Hamilton, Acta Crystallogr. 1955, 8, 199.
29. P. Goldstein, R. A. Jacobsen, J. Am. Chem. Soc. 1962, 84, 2457.
30. The synthesis and properties of this and other 1,3,5,2,4,6-tri- phosphatriboretanes will be described in a forthcoming paper.
31. D. Dou, M. Westerhausen, G. L. Wood, G. Linti, E. N. Duesler, H. Nöth, R. T. Paine, Chem. Ber. 1993, 126, 379.
32. D. Dou, B. Kaufmann, E. N. Duesler, T. Chen, R. T. Paine, H. Nöth, Inorg. Chem. 1993, 32, 3056.
33. S. Lube, R. L. Wells, P. S. White, Inorg. Chem. 1996, 35, 507.
34. T. Chen, E. N. Duesler, R. T. Paine, H. Nöth, Phosphorus, Sulfur, Silicon 1994, 87, 41.
35. T. Chen, E. N. Duesler, R. T. Paine, H. Nöth, Inorg. Chem. 1996, 36, 1070.
36. G. L. Wood, C. K. Narula, E. N. Duesler, R. T. Paine, H. Nöth, J. Chem. Soc. Chem. Commun. 1987, 496.
37. D. Dou, G. L. Wood, E. N. Duesler, R. T. Paine, H. Nöth, Inorg. Chem. 1992, 31, 3756.
38. SMART, Version 5, Bruker Co., Madison.
39. SHELXTL, Version 5, Bruker Co., Madison.