C - S bond activation of two novel asymmetric α-azo- ketenedithioacetals using Fe2(CO)9

Organometallics

Volumn 26, Issue 8, 2007, Pages 1895-1899

  Ortega Alfaro, M Carmen ^a   Alcantara, Olga ^a   Orrala, Manuel ^a   López Cortés, José G ^b   Toscano, Ruben A ^b   Alvarez Toledano, Cecilio ^b  

^a UNIVERSIDAD NACIONAL AUTÓNOMA DE MÉXICO   (Mexico)

^b Instituto de Quimica de la UNAM   (Mexico)

Author keywords

[No Author keywords available]

Indexed keywords

ACTIVATION ENERGY; COMPLEXATION; IRON COMPOUNDS; REACTION KINETICS; STEREOCHEMISTRY; SYNTHESIS (CHEMICAL); X RAY DIFFRACTION ANALYSIS;

DINUCLEAR IRON COMPLEXES; IRON HEXACARBONYL COMPLEXES; TANDEM PROCEDURES;

CHEMICAL BONDS;

EID: 34247529082     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om060953r     Document Type: Article

References (33)

1. For reviews, see: (a) Pearson, A. J. Acc. Chem. Rev. 1980, 13, 463.
2. (b) Pearson, A. J. In Comprehensive Organometallic Chemistry, Vol. 8; Wilkinson, G., Stone, F. G. A., Abel, E. W., Eds.; Pergamon Press: Oxford, 1982; Chapter 58.
3. (c) Pearson, A. J. Metallo-organic Chemistry, Wiley: Chichester, 1985; Chapters 7 and 8.
4. (d) Knölker, H. J. Chem. Soc. Rev. 1999, 28, 151.
5. (e) Ley, S. V.; Cox, L. R.; Meek, G. Chem. Rev. 1996, 96, 423.
6. (f) Pearson, A. J.; Alimardanov, A. Organometallics 1998, 17, 3739.
7. Alvarez-Toledano, C.; Enríquez, J.; Toscano, R. A.; Martínez-García, M.; Cortés-Cortés, E.; Osornio, Y.; García, O.; Gutiérrez-Pérez, R. J. Organomet. Chem. 1999, 577, 38.
8. (a) Ortega-Jiménez, F.; Ortega-Alfaro, M. C.; López- Cortés, J. G.; Velasco-Ibarra, L.; Peña-Cabrera, E.; Alvarez-Toledano, C. Organometallics 2000, 19, 4127.
9. (b) Ortega-Alfaro, M. C.; Lopez-Cortés, J. G.; Toscano, R. A.; Alvarez-Toledano, C. J. Braz. Chem. Soc. 2005, 16, 362-371.
10. Ortega-Alfaro, M. C.; López-Cortés, J. G.; Toscano, R. A.; Alvarez-Toledano, C. J. J. Mex. Chem. Soc. 2005, 49, 124-133.
11. Ortega-Alfaro, M. C.; Hernández, N.; Cerna, I.; López-Cortés, J. G.; Gómez, E.; Toscano, R. A.; Alvarez-Toledano, C. J. Organomet. Chem. 2004, 659, 885-893.
12. Ortega-Alfaro, M. C.; López-Cortés, J. G.; Rangel Sánchez, H.; Toscano, R. A.; Perneres Carrillo, G.; Álvarez- Toledano, C. Arkivoc 2005, vi, 356.
13. 9, frente a ligantes carbonílicos α,β-insaturados. Nuevos arreglos estructurales. Ph.D. Thesis, 2004, UNAM.
14. (a) Hegraly, A. F.; Scott, F. L. J. Org. Chem. 1967, 32, 1957.
15. (b) Hegraly, A. F.; Scott, F. L. J. Chem. Soc (B) 1966, 672.
16. Tronchet, J. M. J.; Baehler, B.; Lehong, N.; Livio, P. F. Helv. Chim. Acta 1971, 54, 921.
17. Tahr, E.; Rupp, H. D. Ann. Chem. 1968, 93, 712.
18. (a) Bailliez, V.; El Kaïm, L.; Michaut, V. Synth. Commun. 2004, 34, 109, and references therein,
19. (b) Allan, V.; El Kaïm, L.; Grimaud, L.; Jana, N. K.; Majee, A. Synlett, 2002, 352.
20. (c) Atlan, V.; Bienaymé, H.; El Kaïm, L.; Majee, A. Chem. Commun. 2000, 1585.
21. (d) Atlan, V.; El Kaim, L.; Supiot, C. Chem. Commun. 2000, 1385.
22. (f) Atlan, V.; El Kaïm, L.; Lacroix, S.; Morgentin, R. Chem. Commun. 1999, 1893.
23. (a) Brown, C. J. Acta Crystallogr. 1966, 21, 146.
24. (b) Chang, C. H.; Porter, R. F.; Baver, S. H. J. Am. Chem. Soc. 1970, 92, 5313.
25. (c) Allmann, R. In PATAI, The Chemistry of Diazonium and Diazo Groups, part 1; Wiley: New York, 1975; p 23.
26. Dieter, R. K. Tetrahedron 1986, 42, 3029.
27. Yates, P.; Lynch, T. R.; Moore, D. R. Can. J. Chem. 1971, 49, 1467.
28. (a) Huges, D. L.; Leigh, G. L.; Paulson, D. Inorg. Chim. Acta 1986, 120, 191.
29. (b) King, R. B. J. Am. Chem. Sac. 1963, 85, 1584.
30. 6a has been synthesized by other methods (see: Winter, A.; Zsolnai, L.; Huttner, G. Z. Z. Naturforsch. Anorg. Chem. 1982, 37B, 1430) and obtained by us as a subproduct from α,β-unsaturated ketone analogues in reactions brought about under similar conditions (ref 3).
31. Braye, E. H.; Hübel, W. Inorg. Synth. 1966, 8, 178.
32. Altomare, A.; Cascarano, G.; Giacovazzo, C.; Guagliardi, A.; Burla, M. C.; Polidori, G.; Canalli, M. J. Appl. Crystallogr. 1994, 27, 435.
33. SHELXTL, version 6.10; Bruker Analytical X-ray Systems: Madison, WI, 2000.