Microstructural and compositional study of a bulk Pb(Mg1/3Nb2/3)O3-PbTiO3 single crystal grown from a BaTiO3 seed

Materials Characterization

Volumn 58, Issue 6, 2007, Pages 534-543

  Samardžija, Zoran ^a   Jeon, Jae Ho ^b   Čeh, Miran ^a  

^a JO EF STEFAN INSTITUTE   (Slovenia)

^b Korea Institute of Machine and Materials   (South Korea)

Author keywords

Compositional homogeneity; Microanalysis; Microstructure; PMNT

Indexed keywords

BARIUM COMPOUNDS; CRYSTAL GROWTH; INTERFACES (MATERIALS); LEAD COMPOUNDS; MICROANALYSIS; SCANNING ELECTRON MICROSCOPY;

COMPOSITIONAL HOMOGENEITY; ORIENTATION ANALYSIS; PMNT;

SINGLE CRYSTALS;

EID: 34247142360     PISSN: 10445803     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.matchar.2006.10.003     Document Type: Article

References (16)

1. Park S.-E., and Shrout T.R. Ultrahigh strain and piezoelectric behaviour in relaxor based ferroelectric single crystals. J Appl Phys 82 4 (1997) 1804-1811
2. 3. J Mater Res 14 8 (1999) 3189-3191
3. 3 single crystals. J Appl Phys 87 5 (2000) 2312-2319
4. Zawilski K.T., Custodio M.C.C., DeMattei R.C., Lee S.-G., Monteiro R.G., Odagawa H., and Feigelson R.S. Segregation during the vertical Bridgman growth of lead magnesium niobate-lead titanate single crystals. J Cryst Growth 258 (2003) 353-367
5. 3 single crystals. Jpn J Appl Phys 41 (2002) 1451-1454
6. Luo H., Xu G., Xu H., Wang P., and Yin Z. Compositional homogeneity and electrical properties of lead magnesium niobate titanate single crystals grown by a modified Bridgman technique. Jpn J Appl Phys 39 (2000) 5581-5585
7. 3 [PMNT] single crystals. J Cryst Growth 209 (2000) 81-90
8. 3 by excess PbO addition. Ferroelectrics 302 (2004) 307-311
9. Lifshin E., and Gauvin R. Minimizing errors in electron microprobe analysis. Microsc Microanal 7 (2001) 168-177
10. Lifshin E., and Gauvin R. The role of Monte Carlo calculations in quantitative analysis. Microsc Microanal 4 (1998) 232-233
11. Hovington P., Drouin D., and Gauvin R. CASINO: a new Monte Carlo code in C language for electron beam interactions - part I: description of the program. Scanning 19 (1997) 1-14
12. Bastin G.F., Dijkstra J.M., and Heijligers H.J.M. PROZA 96: an improved matrix correction program for electron probe microanalysis based on double Gaussian φ(ρz) approach. X-ray Spectrom 27 (1998) 3-10
13. Goldstein JI, Newbury DE, Echlin P, Joy DC, Romig AD, Lyman CE, Fiori C, Lifshin E. Scanning Electron Microscopy and X-Ray Microanalysis. Plenum Press, New York: 1992, (a) p. 417-434; (b) p. 497.
14. Heinrich K.F.J. Mass absorption coefficients for electron probe microanalysis. Proc 11th Int Conf of X-ray Optics and Microanalysis. London, Ontario, Canada, August 4-8 (1987)
15. Marinenko R., and Leigh S. Heterogeneity evaluation of research materials for microanalysis standards certification. Microsc Microanal 10 (2004) 491-506
16. Ziebold T.O. Precision and sensitivity in electron probe microanalysis. Anal Chem 39 (1967) 858-861