-
1
-
-
0038185278
-
-
For reviews, see: a
-
For reviews, see: (a) Sekiguchi, A.; Lee, V. Y. Chem. Rev. 2003, 103, 1429.
-
(2003)
Chem. Rev
, vol.103
, pp. 1429
-
-
Sekiguchi, A.1
Lee, V.Y.2
-
2
-
-
13544249913
-
-
(b) Escudié, J.; Couret, C.; Ranaivonjatovo, H.; Satge, J. Coord. Chem. Rev. 1994, 130, 427.
-
(1994)
Coord. Chem. Rev
, vol.130
, pp. 427
-
-
Escudié, J.1
Couret, C.2
Ranaivonjatovo, H.3
Satge, J.4
-
3
-
-
33748880663
-
-
(c) Driess, M.; Grützmacher, H. Angew. Chem., Int. Ed. Engl. 1996, 35, 828.
-
(1996)
Angew. Chem., Int. Ed. Engl
, vol.35
, pp. 828
-
-
Driess, M.1
Grützmacher, H.2
-
4
-
-
33748240837
-
-
(d) Tsumuraya, T.; Batcheller, S. A.; Masamune, S. Angew. Chem., Int. Ed. Engl. 1991, 30, 902.
-
(1991)
Angew. Chem., Int. Ed. Engl
, vol.30
, pp. 902
-
-
Tsumuraya, T.1
Batcheller, S.A.2
Masamune, S.3
-
5
-
-
33646144694
-
-
(a) Zhu, H.; Oswald, R. B.; Fan, H.; Roesky, H. W.; Ma, Q.; Yang, Z.; Schmidt, H.-G.; Noltemeyer, M.; Starke, K.; Hosmane, N. S. J. Am. Chem. Soc. 2006, 128, 5100.
-
(2006)
J. Am. Chem. Soc
, vol.128
, pp. 5100
-
-
Zhu, H.1
Oswald, R.B.2
Fan, H.3
Roesky, H.W.4
Ma, Q.5
Yang, Z.6
Schmidt, H.-G.7
Noltemeyer, M.8
Starke, K.9
Hosmane, N.S.10
-
6
-
-
23944480318
-
-
(b) Zhu, H.; Chai, J.; Fan, H.; Roesky, H. W.; He, C.; Jancik, V.; Schmidt, H.-G.; Noltemeyer, M.; Merrill, W. A.; Power, P. P. Angew. Chem., Int. Ed. 2005, 44, 5090.
-
(2005)
Angew. Chem., Int. Ed
, vol.44
, pp. 5090
-
-
Zhu, H.1
Chai, J.2
Fan, H.3
Roesky, H.W.4
He, C.5
Jancik, V.6
Schmidt, H.-G.7
Noltemeyer, M.8
Merrill, W.A.9
Power, P.P.10
-
7
-
-
0035913762
-
-
(c) Cui, C.; Köpke, S.; Herbst-Irmer, R.; Roesky, H. W.; Noltemeyer, M.; Schmidt, H.-G.; Wrackmeyer, B. J. Am. Chem. Soc. 2001, 123, 9091.
-
(2001)
J. Am. Chem. Soc
, vol.123
, pp. 9091
-
-
Cui, C.1
Köpke, S.2
Herbst-Irmer, R.3
Roesky, H.W.4
Noltemeyer, M.5
Schmidt, H.-G.6
Wrackmeyer, B.7
-
8
-
-
0000009021
-
-
(d) Uhl, W.; Spies, T.; Koch, R.; Saak, W. Organometallics 1999, 18, 4598.
-
(1999)
Organometallics
, vol.18
, pp. 4598
-
-
Uhl, W.1
Spies, T.2
Koch, R.3
Saak, W.4
-
9
-
-
33645051475
-
-
(e) Li, X.; Song, H.; Duan, L.; Cui, C.; Roesky, H. W. Inorg. Chem. 2006, 45, 1912.
-
(2006)
Inorg. Chem
, vol.45
, pp. 1912
-
-
Li, X.1
Song, H.2
Duan, L.3
Cui, C.4
Roesky, H.W.5
-
10
-
-
4143053604
-
-
(f) Zhu, H.; Chai, J.; Ma, Q.; Jancik, V.; Roesky, H. W.; Fan, H.; Herbst-Irmer, R. J. Am. Chem. Soc. 2004, 126, 10194.
-
(2004)
J. Am. Chem. Soc
, vol.126
, pp. 10194
-
-
Zhu, H.1
Chai, J.2
Ma, Q.3
Jancik, V.4
Roesky, H.W.5
Fan, H.6
Herbst-Irmer, R.7
-
11
-
-
33646924952
-
-
Li, X.; Ni, C.; Song, H.; Cui, C. Chem. Commun. 2006, 1763.
-
(2006)
Chem. Commun
, pp. 1763
-
-
Li, X.1
Ni, C.2
Song, H.3
Cui, C.4
-
12
-
-
4644261519
-
-
Mason, M. R.; Song, B.; Kirschbaum, K. J. Am. Chem. Soc. 2004, 126, 11812.
-
(2004)
J. Am. Chem. Soc
, vol.126
, pp. 11812
-
-
Mason, M.R.1
Song, B.2
Kirschbaum, K.3
-
13
-
-
33751346851
-
-
Li, X.; Duan, L.; Song, H.; Ni, C.; Cui, C. Organometallics 2006, 25, 5665.
-
(2006)
Organometallics
, vol.25
, pp. 5665
-
-
Li, X.1
Duan, L.2
Song, H.3
Ni, C.4
Cui, C.5
-
14
-
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To a solution of LAl[C(O)C(SiMe3)C(SiMe3, 0.13 g, 0.20 mmol) in n-hexane (10 mL) was added a solution of water (1.8 μL, 0.10 mmol) in toluene (2 mL) at -78 °C. The mixture was warmed to room temperature. All volatiles were removed under vacuum, and the remaining solid was crystallized from n-hexane at -20 °C to yield 2 as yellow crystals (0.05 g, 59, Anal. Calcd for C47H77AlN2OSi 4 (825.45, C, 68.39; H, 9.32; N, 3.39. Found: C, 68.31; H, 8.95; N, 3.37. 1H NMR (C6D6, δ -0.02 (s, 18H, SiMe3, 0.51, 0.52 (s, 2 × 9H, SiMe3, 1.00 (d, 6H, J, 6.80 Hz, CHMe2, 1.17 (d, 12H, J, 6.80 Hz, CHMe2, 1.21 (d, 6H, J, 6.80 Hz, 6H, CHMe2, 1.31 (s, 6H, Me, 2.97, 3.09 (sept, 2 × 2H, J, 6.80 Hz, CHMe2, 5.07 (s, 1H, γ-CA, 7.01-7.09 (m, 6H, Ar H, 13C NMR C6D6
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-1 3744 (OH).
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33947701931
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Crystallographic data for 2: Mo Kα (λ, 0.710 73 Å) radiation at 113(2) K, monoclinic, space group P121/n1, a, 11.1041(7) Å, b, 38.623-(2) Å, c, 12.8542(8) Å, β, 115.449(2)°, Z, 4, GOF, 1.061, R1, 0.0481, wR2, 0.1095 for 11 848 reflections (I > 2σI, R1, 0.0583, wR2, 0.1157 for all data. CCDC-620154 contains the supplementary crystallographic data for this paper
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1, a = 11.1041(7) Å, b = 38.623-(2) Å, c = 12.8542(8) Å, β = 115.449(2)°, Z = 4, GOF = 1.061, R1 = 0.0481, wR2 = 0.1095 for 11 848 reflections (I > 2σ(I)); R1 = 0.0583, wR2 = 0.1157 for all data. CCDC-620154 contains the supplementary crystallographic data for this paper.
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(a) Zhu, H.; Chai, J.; He, C.; Bai, G.; Roesky, H. W.; Schmidt, H.-G.; Noltemeyer, M. Organometallics 2005, 24, 380.
-
(2005)
Organometallics
, vol.24
, pp. 380
-
-
Zhu, H.1
Chai, J.2
He, C.3
Bai, G.4
Roesky, H.W.5
Schmidt, H.-G.6
Noltemeyer, M.7
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0037429868
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(b) Bai, G.; Peng, Y.; Roesky, H. W.; Li, J.; Schmidt, H.-G.; Noltemeyer, M. Angew. Chem., Int. Ed. 2003, 42, 1132.
-
(2003)
Angew. Chem., Int. Ed
, vol.42
, pp. 1132
-
-
Bai, G.1
Peng, Y.2
Roesky, H.W.3
Li, J.4
Schmidt, H.-G.5
Noltemeyer, M.6
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18
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0344974254
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Wiberg, K. B.; Dempsey, R. C.; Wendoloski, J. J. J. Phys. Chem. 1984, 88, 5596.
-
(1984)
J. Phys. Chem
, vol.88
, pp. 5596
-
-
Wiberg, K.B.1
Dempsey, R.C.2
Wendoloski, J.J.3
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