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Short reaction times (e.g., 5 min) yield a mixture of 1 and a second product, 2. The second product can be removed by recrystallization of crude 1 from THF or avoided altogether by using longer reaction times. The formation and chemistry of 2 is still under investigation.
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Acyl coordination to the aluminum atoms in 1 is sufficiently robust that crystallization from THF does not give THF-solvated monomers.
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