The real nature of the indole alkaloids in Cortinarius infractus: Evaluation of artifact formation through solvent extraction method development

Journal of Chromatography A

Volumn 1148, Issue 1, 2007, Pages 1-7

  Brondz, Ilia ^a   Ekeberg, Dag ^a   Høiland, Klaus ^b   Bell, David S ^c   Annino, Amy R ^d  

^a NORWEGIAN UNIVERSITY OF LIFE SCIENCES   (Norway)

^b UNIVERSITY OF OSLO   (Norway)

^c Supelco Inc   (United States)

^d PENNSYLVANIA STATE UNIVERSITY   (United States)

Author keywords

Carboline 1 propionic acid; 6 Hydroxy carboline 1 propionic acid; Artifacts of indole alkaloids; Chemotaxonomy; Cortinarius infractus; HPLC MS; pre infractine; Revision of extraction procedure; Separation of alkaloids on Discovery ZR PS HPLC column

Indexed keywords

6-HYDROXY-Β-CARBOLINE-1-PROPIONIC ACID; ALKALOIDS; CARBOLINE-1-PROPIONIC ACID; CHEMOTAXONOMY; CORTINARIUS INFRACTUS; EXTRACTION PROCEDURE; INDOLE ALKALOIDS;

HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; METHANOL; NITROGEN COMPOUNDS; PLANTS (BOTANY); SOLVENT EXTRACTION;

AROMATIC COMPOUNDS;

6 HYDROXYINFRACTINE; BETA CARBOLINE 1 PROPIONIC ACID; BIOCHEMICAL MARKER; INDOLE ALKALOID; INFRACTINE; METHANOL; PROPIONIC ACID DERIVATIVE; UNCLASSIFIED DRUG;

AGARICALES; ARTICLE; ARTIFACT; CHEMOTAXONOMY; CORTINARIUS; CORTINARIUS INFRACTUS; EVALUATION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; MUSHROOM; NONHUMAN; PRIORITY JOURNAL; SOLVENT EXTRACTION; TECHNIQUE;

AGARICALES; ARTIFACTS; CARBOLINES; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; INDOLE ALKALOIDS; METHANOL; MODELS, THEORETICAL; MOLECULAR STRUCTURE; PROPIONIC ACIDS; SOLVENTS; TANDEM MASS SPECTROMETRY;

AGARICALES; BASIDIOMYCOTA; CORTINARIUS INFRACTUS;

EID: 33947637215     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2007.02.074     Document Type: Article

References (12)

1. Steglich W., Kopanski L., Wolf M., Moser M., and Tegtmeyer G. Tetrahedron. Lett. 25 (1984) 2341
2. Yang J.S., and Gong D. Benn. Acta Chim. Sinica 42 7 (1984) 679
3. Brondz I., Høiland K., Bell D.S., and Annino A.R. TheReporter, Supelco 24 3 (2006) 6
4. I. Brondz, A.R. Annino, K. Høiland, J. Chromatogr. A. (2007), submitted for publication
5. Brondz I. Anal. Chim. Acta 465 (2002) 1
6. Brondz I. Fatty Acids. In: Worsfold P.J., Townshend A., and Poole C.F. (Eds). Encyclopedia of Analytical Science. second ed. (2004), Elsevier, Academic Press 76
7. International Union of Pure and Applied Chemistry, Division of Organic Chemistry, Commission on Nomenclature of Organic Chemistry, A Guide to IUPAC Nomenclature of Organic Compounds, Recommendations 1993, R. Panico, W.H. Powell, J-C. Richer (Eds.), Blackwell Scientific Publications, Oxford, U.K. (1993).
8. In: Silverstein R.M., Bassler G.C., and Morrill T.C. (Eds). Spectrometric Identification of Organic Compounds (1981), John Wiley, Sons, New York, Chichester, Brisbane, Toronto 27-29
9. Pelletier S.W. In: Pelletier S.W. (Ed). Chemistry of the alkaloids (1970), Van Norstrand Reinhold Company, New York, Cincinnati, Toronto, London, Melbourne 1
10. Waller G.R., and Nowacki E.K. in Alkaloid Biology and Metabolism in Plants (1978), Plenum Press, New York and London pp. 15-16
11. I. Brondz, K. Høiland, J. Lefler, Supercritical fluid chromatography resolution of secondary metabolites and multi-analysis by mass spectrometry-ultraviolet and corona charged aerosol detection, 12 Norske seminar i massespektrometri (Norway) Hafjell 21-24 January 2007. abstr. p. 63.
12. Bracher F., and Hildebrand D. Pharmazie 50 3 (1995) 182