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Crystal data for {MnII⊂[MnII2Mn III4Cl6(L3)6, 4, 4·2CHCl3: C48H 102Cl6Mn7N6O12· 2CHCl3, M, 1791.37 g mol-1; crystal dimensions 0.30 x 0.30 x 0.20 mm3; triclinic, space group P1, a, 11.8080(2) Å, b, 13.3640(3) Å, c, 13.7280(3) Å, α, 70.2460(10)°, β, 67.2800(10)°, γ, 71.3640(10)°, V, 1835.50(7) Å3; Z, 1; F(000, 921, ρcalcd, 1.621 g cm-3; Nonius KappaCCD diffractometer, Mo Kα radiation (λ, 0.710 73 Å, T, 173(2) K; graphite monochromator; Θ range [deg] 2.24 < Θ < 27.52; section of the reciprocal lattice, 15 ≤ h ≤ 15, 17 ≤ k ≤ 17, 17 ≤
-
14c,15 Disorder: C6/C6′ = 48:52 and C8/C8′ = 52:48; all of the solvent molecules (three THF) are disordered.
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56
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33947389799
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SHELXTL NT 6.12; Bruker AXS, Inc.: Madison, WI, U.S.A., 2002.
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(c) SHELXTL NT 6.12; Bruker AXS, Inc.: Madison, WI, U.S.A., 2002.
-
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57
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33947419475
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3] and CCDC 271408 [(4)·3THF] contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from the Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.
-
3] and CCDC 271408 [(4)·3THF] contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from the Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.
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For further details compare with information in Supporting Information
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For further details compare with information in Supporting Information.
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