A morphological study of poly[bis(trifluoroethoxy)phosphazene] using solid-state NMR: Introducing domain selective 1H and 19F decoupled 13C MAS NMR

Journal of Inorganic and Organometallic Polymers and Materials

Volumn 16, Issue 4, 2006, Pages 343-357

  Hazendonk, Paul ^a   DeDenus, Christine ^b   Iuga, Adriana ^a   Cahoon, Philip ^a   Nilsson, Ben ^a   Iuga, Dinu ^a  

^a UNIVERSITY OF LETHBRIDGE   (Canada)

^b HOBART AND WILLIAM SMITH COLLEGES   (United States)

Author keywords

DIVAM; MAS NMR; Phosphazenes; Poly bis(trifluoroethoxy)phosphazene

Indexed keywords

EID: 33847377076     PISSN: 15741443     EISSN: 15741451     Source Type: Journal    
DOI: 10.1007/s10904-006-9061-8     Document Type: Article

References (56)

1. H. R. Allcock, Chemistry and Application of Polyphosphazenes (Wiley & Sons, New York, 2003).
2. J. E. Mark, H. R. Allcock, and R. West, Inorganic Polymers (Prentice Hall, Englewood Cliffs, New Jork, 1992).
3. R. H. Neilson and P. Wisian-Nielson, Chem. Rev. 88, 541 (1988).
4. C. H. Honeyman, I. Manners, C. T. Morrissey, and H. R. Allcock, J. Am. Chem. Soc. 1117, 7035 (1995).
5. H. R. Allcock, J. M. Nelson, C. R. Denus, and I. Manners, Tailored Polymers and Applications (VSP International Science Publishers, Netherlands, 2000).
6. J. M. Nelson, H. R. Allcock, and I. Manners, Macromolecules 30, 3191 (1997).
7. A. J. Bur, in Fluoropolymers, L. A. Wall, ed. (Wiley, New York, 1972).
8. H. R. Allcock, C. R. Denus, R. Prange, and J. R. Nelson, Macromolecules 32, 7999 (1999).
9. G. Tesi and C. M. Douglas, J. Chem. Soc. 549 (1962).
10. S. G. Young and J. M. Magill, Macromolecules 22, 2549 (1989).
11. S. G. Young, M. Kojima, J. H. Magill, and F. T. Lin, Phase Trans Polyphosphazene 15, 3215 (1992).
12. N. S. Schneider, C. R. Desper, and R. E. Singler, J. Appl. Polym. Sci. 20, 3087 (1976).
13. M. Kojima and J. H. Magill, Makromol. Chem. 186, 649 (1985).
14. M. Kojima and J. M. Magill, Polymer 26, 1971 (1985).
15. P. Mourik, E. Veldman, B. Norder, J. Turnhout, and M. Wuebbenhorst, J. Mater. Sci. 40, 1661 (2005).
16. R. J. Ciora and J. H. Magill, Macromolecules 23, 2350 (1990).
17. M. H. Levitt, Spin Dynamics, Basics of Magnetic Resonance (John Wiley & Sons Ltd., Chichester, England, 2001).
18. E. R. Andrew, A. Bradbury, and R. G. Eades, Nature 182, 1659 (1958).
19. I. J. Lowe, Phys. Rev. Lett. 2, 258 (1959).
20. A. Pines, M. G. Gibby, and J. S. Waugh, J. Chem. Phys. 59, 569 (1973).
21. S. R. Hartmann and E. L. Hahn, Phys. Rev. 128, 2042 (1962).
22. A. Pines, M. G. Gibby, and J. S. Waugh, J. Chem. Phys. 56, 1776 (1972).
23. A. E. Bennet, C. M. Rienstra, M. Auger, K. V. Lakshmi, and R. G. Griffin, J. Chem. Phys. 103, 6951 (1995).
24. E. O. Stejskal, J. Schaefer, and J. S. Waugh, J. Magn. Reson. 28, 105 (1977).
25. C. Luchinat, M. Piccioli, R. Pierattelli, F. Engelke, T. Marquardsen, and R. Ruin, J. Magn. Reson. 150(2), 161 (2001).
26. R. Hill, A. Calver, S. Skinner, A. Stamboulis, and R. Law, Key Eng. Mater. 309-311, 305 (2006).
27. K. M. Miller, Progress in NMR Spectroscopy 28, 255 (1996).
28. R. K. Harris and P. Jackson, Chem. Rev. 91, 1427 (1991).
29. S. Ando, R. K. Harris, and U. Scheler, Encyclopedia of NMR, Advances in NMR, Vol. 9 (John Wiley and Sons Ltd., Chichester, 2002), pp. 531-550.
30. H. R. Allcock, J. M. Nelson, S. D. Reeves, C. H. Honeyman, and I. Manners, Macromolecules 30, 50 (1997).
31. A. Comotti, M. C. Gallazzi, R. Simonutti, and P. Sozzani, Chem. Mater. 10, 3589 (1998).
32. R. Simonutti, W. S. Veeman, F. C. Ruhnau, M. C. Gallazzi, and P. Sozzani, Macromolecules 29, 4958 (1996).
33. R. C. Crosby and J. F. Haw, Macromolecules 20, 2326 (1987).
34. R. C. Crosby, J. F. Haw, and D. H. Lewis, Anal. Chem. 60, 2695 (1988).
35. H. Tanaka, M. A. Gomez, A. E. Tonelli, S. V. Chichester-Hicks, and R. C. Haddon, Macromolecules 22, 1031 (1989).
36. H. Tanaka, M. A. Gomez, A. E. Tonelli, S. V. Chichester-Hicks, and R. C. Haddon, Macromolecules 21(7), 2301 (1988).
37. S. V. Meille, A. Farina, M. C. Gallazi, P. Sozzani, R. Simonutti, and A. Comotti, Macromolecules 28, 1893 (1995).
38. R. Simonutti, A. Comotti, and P. Sozzani, J Inorg Organ Polym 6(4), 313 (1996).
39. H. R. Allcock, G. Cameron, T. W. Skloss, S. Taylor-Meyers, and J. F. Haw, Macromolecules 29, 233 (1996).
40. S. A. Taylor, J. L. White, N. C. Elbaum, R. C. Crosby, G. C. Campbell, J. F. Haw, and G. R. Hatfield, Macromolecules 25, 3369 (1992).
41. K. Takegoshi, I. Tanaka, K. Hickichi, and S. Higashida, Macromolecules 25, 3392 (1992).
42. C. Kim and H. R. Allcock, Macromolecules 20, 1727 (1987).
43. M. N. Alexander, C. R. Desper, P. L. Sagalyn, and N. S. Schneider, Macromolecules 10(3), 721 (1977).
44. R. Graf, D. E. Demco, J. Gottwald, S. Hafner, and H. W. Spiess, J. Chem. Phys. 106, 885 (1997).
45. A. Kenwright, B. J. Say, in NMR Spectroscopy of Polymers, R. N. Ibbett, ed. (Blackie Academic and Professional, Glasgow 1993), pp. 231-274.
46. S. J. Opella and M. H. Frey, J. Am. Chem. Soc. 102, 5854 (1979).
47. U. Scheler and R. K. Harris, Solid State NMR 7, 11 (1996).
48. X.-P. Tang, K. C. Chartkunchand, and Y. Wu, Chem. Phys. Lett. 399(4-6), 456 (2004).
49. D. J. Harris, E. R. Azevedo, and T. J. Bonagamba, J. Magn. Reson. 162, 67 (2003).
50. P. Wormald, D.C. Apperley, F. Beaume, and R. K. Harris, Polymer 44(3), 643 (2003).
51. N. Egger, K. Schmidt-Rohr, B. Blumich, W. D. Domke, and B. Stapp, J. Appl. Polym. Sci. 44, 289 (1992).
52. J.-D. Mao and K. Schmidt-Rohr, Solid State NMR 26, 36 (2004).
53. S. Ando, R. K. Harris, P. Hazendonk, and P. Wormald, Macromol. Rapid Commun. 26, 345 (2005).
54. M. Kojima, W. Kluge, and J.H. Magill, Macromolecules 17, 1421 (1984).
55. S. F. Liu and K. Schmidt-Rohr, Macromolecules 34, 8416 (2001).
56. E. Vinogradov, P. K. Madhu, and S. Vega, Chem. Phys. Lett. 314, 443 (1999).